A kind of preparation method of cotton cellulose nanofibril film
A technology of nanofibrils and cotton fibers, which is applied in the fields of pulping of cellulose raw materials, post-treatment of cellulose pulp, and treatment of cellulose with microorganisms/enzymes. High cost and other issues, to achieve the effect of low cost, cost reduction, and production cost reduction
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Embodiment 1
[0029] A preparation method of cotton cellulose nanofibril film, comprising the following steps:
[0030] (1) Wash the cotton raw material with water to remove impurities, dry it and place it in a hydrothermal reaction kettle, add 1mmol / L hydrochloric acid solution that is 8 times the mass of the cotton raw material, heat up to 150°C for 60 minutes of hydrolysis reaction, and then wash the acid with water and blow it Dry, then add the hydrolyzed and dried cotton raw materials, sodium hydroxide, sodium sulfide and water into the reaction kettle according to the mass ratio of 10:4:4:100, boil in alkali at 160°C for 120 minutes, filter and wash The obtained product is then mixed with sodium chlorite, acetic acid, and water in a mass ratio of 8:3:2:300, and reacted at 70°C for 120 minutes. After completion, the obtained product is washed with water, and the cotton fiber pulp is obtained after suction filtration;
[0031] (2) Add the cotton fiber pulp obtained in step 1 into 12 tim...
Embodiment 2
[0037] A preparation method of cotton cellulose nanofibril film, comprising the following steps:
[0038] (1) Wash the cotton raw material with water to remove impurities, dry it and put it in a hydrothermal reaction kettle, add 1mmol / L hydrochloric acid solution 10 times the mass of the cotton raw material, heat up to 170°C for 40 minutes, and then wash the acid with water and blow it Dry, then add the hydrolyzed and dried cotton raw materials, sodium hydroxide, sodium sulfide and water into the reaction kettle according to the mass ratio of 12:5:5:100, boil in alkali at 180 °C for 90 minutes, filter and wash The obtained product is then mixed with sodium chlorite, acetic acid, and water in a mass ratio of 10:3.5:3:320, and reacted at 80°C for 90 minutes. After completion, the obtained product is washed with water, and the cotton fiber pulp is obtained after suction filtration;
[0039] (2) adding the cotton fiber pulp obtained in step 1 into water of 18 times the mass, dilut...
Embodiment 3
[0045] A preparation method of cotton cellulose nanofibril film, comprising the following steps:
[0046] (1) Wash the cotton raw material with water to remove impurities, dry it and place it in a hydrothermal reaction kettle, add 1mmol / L hydrochloric acid solution of 9 times the mass of the cotton raw material, heat up to 160°C for 50 minutes of hydrolysis reaction, and then wash the acid with water and blow it Dry, then add the hydrolyzed and dried cotton raw materials, sodium hydroxide, sodium sulfide and water into the reaction kettle according to the mass ratio of 11:4.5:4.5:100, boil in alkali at 170°C for 105 minutes, filter and wash The obtained product is then mixed with sodium chlorite, acetic acid, and water in a mass ratio of 9:3.5:2:310, and reacted at 75°C for 105 minutes. After completion, the obtained product is washed with water, and the cotton fiber pulp is obtained after suction filtration;
[0047] (2) adding the cotton fiber pulp obtained in step 1 into 15...
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