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High-iron low-copper samarium-cobalt permanent magnet material and preparation method thereof

A permanent magnet material and high-speed iron technology, applied in the direction of magnetic material, inductor/transformer/magnet manufacturing, magnetic objects, etc., can solve the problems of comprehensive magnetic performance reduction, coercive force deterioration, etc., achieve short aging time and improve powder output efficiency , The effect of reducing manufacturing costs

Active Publication Date: 2020-04-10
福建省长汀卓尔科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] When the existing magnetic steel Fe content mentioned in the above-mentioned background technology is higher than 25%, although the residual magnetic energy reaches 12KGs, its coercive force deteriorates very seriously, and the problem that the comprehensive magnetic performance reduces, the present invention provides a kind of The high-iron and low-copper type samarium cobalt permanent magnet material includes the following components by mass fraction:

Method used

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  • High-iron low-copper samarium-cobalt permanent magnet material and preparation method thereof
  • High-iron low-copper samarium-cobalt permanent magnet material and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0030] Raw materials: samarium, cobalt, iron, copper, zirconium

[0031] The mass percentages of the above raw materials are compounded: 24.5% of samarium, 46% of cobalt, 25% of iron, 2% of copper and 2.5% of zirconium.

[0032] The specific preparation method is as follows:

[0033] Step 1: Batching and Melting

[0034] Put samarium, cobalt, iron, copper, and zirconium in a certain order into the crucible of the vacuum quick-setting belt furnace, and the order of stacking from bottom to top is: cobalt-zirconium-iron-copper- samarium. After vacuum smelting, refining and heat preservation, it is poured on a water-cooled copper roller, and after cooling, a quick-setting strip sheet is obtained. The rotational speed of the copper roller is controlled at 30 rpm, and the average thickness of the strip strip produced is 1 mm.

[0035] Step 2: Homogenization

[0036]The quick-setting fling strips were vacuum-insulated in a vacuum furnace, the homogenization treatment temperature...

Embodiment 2

[0044] Raw materials: samarium, cobalt, iron, copper, zirconium

[0045] The mass percentages of the above raw materials are compounded: 25.2% of samarium, 44% of cobalt, 26% of iron, 2.3% of copper and 2.5% of zirconium.

[0046] The specific preparation method is as follows:

[0047] Step 1: Batching and Melting

[0048] Put samarium, cobalt, iron, copper, and zirconium in a certain order into the crucible of the vacuum quick-setting belt furnace. The order of stacking from bottom to top is: cobalt-zirconium-iron-copper- samarium. After vacuum smelting, refining and heat preservation, it is poured on a water-cooled copper roller, and after cooling, a quick-setting strip sheet is obtained. The rotational speed of the copper roller was controlled at 28 rpm, and the average thickness of the strip strip produced was 1.2mm.

[0049] Step 2: Homogenization

[0050] The quick-setting fling strips are vacuum-insulated in a vacuum furnace, the homogenization treatment temperatur...

Embodiment 3

[0058] Raw materials: samarium, cobalt, iron, copper, zirconium

[0059] The mass percentages of the above raw materials are compounded: 25% of samarium, 42% of cobalt, 28% of iron, 2.5% of copper and 2.5% of zirconium.

[0060] The specific preparation method is as follows:

[0061] Step 1: Batching and Melting

[0062] Put samarium, cobalt, iron, copper, and zirconium in a certain order into the crucible of the vacuum quick-setting belt furnace. The order of stacking from bottom to top is: cobalt-zirconium-iron-copper- samarium. After vacuum smelting, refining and heat preservation, it is poured on a water-cooled copper roller, and after cooling, a quick-setting strip sheet is obtained. The rotational speed of the copper roller was controlled at 25 rpm, and the average thickness of the strip sheet was 1.5 mm.

[0063] Step 2: Homogenization

[0064] The quick-setting fling strips are vacuum-insulated in a vacuum furnace, the homogenization treatment temperature is 980 °...

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Abstract

The invention relates to the technical field of rare earth permanent magnet materials, in particular to a high-iron low-copper samarium-cobalt permanent magnet material and a preparation method thereof, and the high-iron low-copper samarium-cobalt permanent magnet material comprises the following components in percentage by mass: 21%-26% of samarium, 42%-46% of cobalt, 25%-28% of iron, 2%-2.5% ofcopper and 2%-3% of zirconium. The preparation method of the high-iron low-copper samarium-cobalt permanent magnet material comprises the following preparation steps of burdening and smelting, homogenization treatment, coarse crushing, airflow powder grinding and forming, sintering solid solution and aging. According to the high-iron low-copper samarium-cobalt permanent magnet material provided bythe invention, a rapid hardening melt-spinning sheet with high iron content is subjected to homogenization treatment, the samarium-cobalt magnetic steel with the residual magnetism being 11.7 KGs orabove, the intrinsic coercive force being 25 KOe or above and the magnetic energy product being 31 MGOe or above can be stably prepared, the magnetic performance reaches the international advanced level, large-scale industrial production can be conducted, and the domestic production level is broken through.

Description

technical field [0001] The invention relates to the technical field of rare earth permanent magnet materials, in particular to a high iron and low copper type samarium cobalt permanent magnet material and a preparation method thereof. Background technique [0002] Samarium cobalt permanent magnet material belongs to the first generation rare earth permanent magnet material. Compared with Nd-Fe-B, it has high service temperature and good corrosion resistance, but its magnetic energy product is relatively low. Since the 1960s, scientific researchers have done a lot of research on improving the magnetic energy product. In order to increase the magnetic energy product, it is mainly to increase the remanence and coercive force of the magnet. Studies have shown that increasing the Fe content in the formula or reducing the Cu content in the formula can effectively increase the remanence, and at the same time increase the coercive force of the magnet through appropriate heat treatm...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01F1/057H01F41/02
CPCH01F1/0577H01F41/0266
Inventor 范荣辉王国雄傅忠伟陈李泽方
Owner 福建省长汀卓尔科技股份有限公司