Organic microsphere with blue-green alga removing function and preparation method thereof
A production method and organic technology, applied in the field of water purification, which can solve the problems of sinking to the bottom, affecting the function and so on.
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Embodiment 1
[0026] A method for making organic microspheres with the function of removing cyanobacteria, comprising the steps of:
[0027] (1) dissolving sodium alginate and polyglutamic acid in water to obtain a mixed solution of sodium alginate and polyglutamic acid; the mass ratio of sodium alginate, polyglutamic acid and water is: 1:5:200;
[0028] (2) After 0.15g of graphene oxide is placed in 50ml of deionized water and ultrasonically dispersed for 2h, it is added to the sodium alginate and polyglutamic acid mixed solution of step (1), and the graphene oxide aqueous solution and sodium alginate, The ratio of polyglutamic acid mixed solution is 1:1, then diatomite and bentonite are added, ultrasonically stirred for 25min, the ratio of diatomite, bentonite and graphene oxide is 5:3:1 to obtain a mixture;
[0029] (3) the mixture of step (2) is dripped in the calcium chloride fixative solution and reacted for 60min, and after the reaction is completed, wash with deionized water for 2 t...
Embodiment 2
[0033] A method for making organic microspheres with the function of removing cyanobacteria, comprising the steps of:
[0034] (1) dissolving sodium alginate and polyglutamic acid in water to obtain a mixed solution of sodium alginate and polyglutamic acid; the mass ratio of sodium alginate, polyglutamic acid and water is: 2:6:280;
[0035] (2) After 0.15g of graphene oxide is placed in 50ml of deionized water and ultrasonically dispersed for 2h, it is added to the sodium alginate and polyglutamic acid mixed solution of step (1), and the graphene oxide aqueous solution and sodium alginate, The ratio of polyglutamic acid mixed solution is 1:1, then diatomite and bentonite are added, ultrasonically stirred for 5-30min, the ratio of diatomite, bentonite and graphene oxide is 5:3:1, and the mixture is obtained;
[0036] (3) the mixture of step (2) is dripped in the calcium chloride fixative solution and reacted for 120min, after the reaction is completed, wash with deionized water...
Embodiment 3
[0040] A method for making organic microspheres with the function of removing cyanobacteria, comprising the steps of:
[0041] (1) dissolving sodium alginate and polyglutamic acid in water to obtain a mixed solution of sodium alginate and polyglutamic acid; the mass ratio of sodium alginate, polyglutamic acid and water is: 5:8:300;
[0042] (2) After 0.15g of graphene oxide is placed in 50ml of deionized water and ultrasonically dispersed for 2h, it is added to the sodium alginate and polyglutamic acid mixed solution of step (1), and the graphene oxide aqueous solution and sodium alginate, The ratio of polyglutamic acid mixed solution is 1:1, then diatomite and bentonite are added, ultrasonically stirred for 5-30min, the ratio of diatomite, bentonite and graphene oxide is 5:3:1, and the mixture is obtained;
[0043] (3) drop the mixture of step (2) into the calcium chloride fixative solution and react for 30~120min. The content is 15g / L, and the volume ratio of the mixture to...
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