A kind of cnts reinforced magnesium-based composite material and preparation method thereof

A technology of composite materials and magnesium ingots is applied in the field of preparation of magnesium-based composite materials, which can solve the problems of limited development and reduced elongation, and achieve the effects of strict procedures, improved strength, and significantly finer grains.

Active Publication Date: 2021-04-23
SHAANXI UNIV OF SCI & TECH
View PDF9 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

When the CNTs reinforced magnesium matrix composites prepared by the traditional direct addition method obtain high tensile strength and yield strength, the elongation will decrease, which limits the application and development of magnesium matrix composites as structural materials in the engineering field.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • A kind of cnts reinforced magnesium-based composite material and preparation method thereof
  • A kind of cnts reinforced magnesium-based composite material and preparation method thereof
  • A kind of cnts reinforced magnesium-based composite material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0029] The present invention will be described in detail below in conjunction with specific embodiments and accompanying drawings.

[0030] The preparation process of CNTs / Mg-6Zn composite material of the present invention is as follows:

[0031] S1, Pretreatment of CNTs

[0032] Carbon nanotubes (CNTs) have strong van der Waals forces and relatively large areas, so pristine CNTs generally exist in the form of winding and agglomeration. The present invention purifies CNTs (concentrated sulfuric acid and concentrated nitric acid mixed acid solution with a volume ratio of three to one), which can effectively remove amorphous carbon and impurities therein; the present invention weighs 6g of original CNTs;

[0033] CNTs will be lost after pretreatment, and the loss ratio is about 25%. The present invention weighs 0.5vol% of CNTs after pickling, and the weighing amount is 4.08g;

[0034] S2, preparing magnesium alloy semi-solid slurry:

[0035] First, raise the temperature of th...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
hardnessaaaaaaaaaa
tensile strengthaaaaaaaaaa
hardnessaaaaaaaaaa
Login to view more

Abstract

The invention discloses a CNTs-reinforced magnesium-based composite material and a preparation method thereof. The CNTs are pre-dispersed by a chemical pretreatment method, and the CNTs-reinforced magnesium-based composite material is prepared by a stirring casting method. The results show that the chemical pretreatment composite stirring The casting method has a positive effect on the uniform dispersion of CNTs; the present invention aims at the poor wettability of CNTs on the metal interface, and the phenomenon that agglomeration easily occurs in the metal melt, and the magnesium alloy is used as the matrix and the CNTs are used as reinforcements. The CNTs / Mg-6Zn composite material is made after semi-solid stirring smelting, ultrasonic-assisted stirring, casting, solid solution and aging treatment under the action of the atmosphere. This preparation method has advanced technology and strict procedures. The prepared CNTs / Mg6ZnCNTs / Mg ‑6Zn composite material, after adding CNTs, the structure of CNTs / Mg‑6Zn composite material is more refined, and the grain size is obviously finer, which realizes fine grain strengthening; near the grain boundary of CNTs / Mg‑6Zn composite material, it can be found that With multiple second phases, CNTs hinder the movement of dislocations, resulting in the accumulation of dislocations, which plays a role in strengthening the second phase.

Description

technical field [0001] The invention belongs to the field of preparation of magnesium-based composite materials, and in particular relates to a CNTs-reinforced magnesium-based composite material and a preparation method thereof. Background technique [0002] In recent years, magnesium matrix composites (MMCs) have attracted the attention of a large number of researchers due to their ultra-lightweight, high specific strength and high specific stiffness. At the same time, magnesium-based composite materials have extremely broad application prospects in the fields of aerospace and automobile manufacturing. The performance of magnesium-based composites can be enhanced by adding specific reinforcing materials. Carbon nanotubes (CNTs), as novel one-dimensional nanomaterials, have attracted considerable attention due to their unique mechanical, electrical, and thermal properties as well as low density and already extensive research interest. In recent years, researchers have begu...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Patents(China)
IPC IPC(8): C22C1/10C22C1/02C22C23/04C22F1/06
CPCC22C1/1036C22C23/04C22C26/00C22C2026/002C22F1/06
Inventor 沈明杰李云帅朱小倩
Owner SHAANXI UNIV OF SCI & TECH
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products