Digestion solution for digesting organic impurities in micro-plastics, preparation method of digestion solution and digestion method based on digestion solution
A technology of organic impurities and digestion solution, which is applied in the field of impurity treatment in microplastics. It can solve the problems of device system impact, ineffective application, and experimental danger, etc., achieve high digestion rate, and alleviate the difficulty of qualitative detection of microplastics.
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[0059] According to one aspect of the present invention, a kind of preparation method of above-mentioned digestion liquid, described preparation method comprises the following steps:
[0060] Mixing an aqueous solution of potassium persulfate and an aqueous solution of an alkaline compound to obtain a digestion solution, the concentration of potassium persulfate in the digestion solution is 0.1-0.35 mol / L, and the concentration ratio of potassium persulfate and alkaline compound is 1:1-3;
[0061] The preparation method of the above-mentioned digestion liquid provided by the present invention, the above-mentioned method is to mix potassium persulfate aqueous solution and alkaline compound aqueous solution to obtain digestion liquid, the concentration of potassium persulfate in the digestion liquid is 0.1~0.35mol / L, potassium persulfate Concentration ratio with basic compound is 1:1~3. The above preparation method has a simple process and is easy to operate.
[0062] In the ab...
Embodiment 1
[0087] A digestion solution for digesting organic impurities in microplastics, the preparation method of the digestion solution comprises the following steps:
[0088] (a) When preparing 1L of digestion solution, dissolve 27g of potassium persulfate in 700-800mL of deionized water at about 30°C, dissolve 8g of sodium hydroxide in 50-100mL of deionized water and cool to prepare persulfuric acid Potassium solution and sodium hydroxide solution;
[0089] (b), the potassium persulfate solution obtained in step (a) is mixed with sodium hydroxide solution to obtain a mixed solution, and the concentration of potassium persulfate in the mixed solution is adjusted to 0.1mol / L, and the concentration of sodium hydroxide is 0.2mol / L L, made the digestion solution;
[0090] The mixing temperature of the potassium persulfate solution and the alkaline compound solution in the step (b) is 10-30°C.
Embodiment 2
[0092] A digestion solution for digesting organic impurities in microplastics, the preparation method of the digestion solution comprises the following steps:
[0093] (a) When preparing 1L of digestion solution, dissolve 94.5g of potassium persulfate in 700-800mL of deionized water at about 30°C, dissolve 14g of sodium hydroxide in 50-100mL of deionized water and cool to prepare over Potassium sulfate solution and sodium hydroxide solution;
[0094](b), the potassium persulfate solution obtained in step (a) is mixed with sodium hydroxide solution to obtain a mixed solution, and the concentration of potassium persulfate in the mixed solution is adjusted to 0.35mol / L, and the concentration of sodium hydroxide is 0.35mol / L L, made the digestion solution;
[0095] The mixing temperature of the potassium persulfate solution and the alkaline compound solution in the step (b) is 10-30°C.
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