Food composition or feed composition containing epoxy group-removed protease and processing method of food composition or feed composition
A technology of feed composition and processing method, applied in the field of diet or feed composition
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[0056] 1. The active polypeptide FTCD catalyzes the removal of epoxy groups from trichothecenes
[0057] 1. Experimental method:
[0058] 1.1 In vitro enzymatic reaction:
[0059] Dissolve DON, 3-DON, 15-ADON, NIV, DAS, HT-2, T-2 toxins (1 mg) in freshly prepared GSH (30.7 mg, 100 μmol) in PBS buffer, and add active peptides, Insulate in a 20°C water bath for 24 hours.
[0060] 1.2 LC-HRMS ( / MS) analysis
[0061] After the in vitro reaction solution was filtered through a 0.22 μm filter membrane, it was transferred to an injection vial for LC-HRMS detection. LC-HRMS( / MS) Analysis Data were analyzed using Xcalibur 2.1.0. The extracted ion chromatograms (EIC) of the toxin and its derivatives were studied using the peak shape, retention time (±0.2 min) and mass (±5 ppm) of the proposed biotransformation products. According to the secondary spectrum and the basic structure of the substance, the neutral loss is analyzed, and the chemical structure is deduced.
[0062] 2. Expe...
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