Ganaxolone for use in treating genetic epileptic disorders
A technology of ganaxolone and epilepsy, applied in the field of ganaxolone for the treatment of hereditary epilepsy
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[0527] The following examples of formulations according to the invention should not be construed as limiting the invention in any way, but merely as samples of the various formulations described herein.
example 1
[0530] A 50 mg / ml ganaxolone suspension was prepared having the composition listed in Table 1 below:
[0531] Table 1: Composition of 50mg / ml Ganaxolone Suspension
[0532]
[0533]
[0534] Table 2 shows the function of the excipients used in the 50 mg / ml ganaxolone suspension.
[0535] Table 2: Summary of Component Functions for 50mg / ml Ganaxolone Suspension
[0536]
[0537] The oral bioavailability of 50 mg / ml ganaxolone suspension depends on the rate and extent of nanoparticle drug dissolution in the relevant physiological environment. The method and specification for granulation shaping are designed to ensure that the ganaxolone drug product does not exhibit aggregation after dispersion in simulated gastrointestinal fluids.
[0538] Figure 3B A summary of the key steps in the suspension manufacturing process applicable to the 50 mg / ml ganaxolone suspension is provided.
[0539] The dispersion nanomilling process was used to reduce the particle size of ganax...
example 2
[0546] Ganaxolone capsules (225 mg) were prepared with the ingredients listed in Tables 4 and 5 below:
[0547] Table 4: Composition of 225 mg Ganaxolone Capsules IR Beads
[0548]
[0549] Table 4: Composition of 225 mg Ganaxolone Capsules IR Beads
[0550] Element grade %w / w Ganaxolone GMP 45.06 Hydroxypropylmethylcellulose (Pharmacoat 603) USP / EP 10.28 Sodium dodecyl sulfate USP / EP / NF 0.70 Sodium Methylparaben USP 0.26 sodium benzoate USP / EP 0.20 Citric acid, anhydrous USP / EP 0.39 Sodium chloride USP / EP 1.03 30% Simethicone Emulsion, (Dow Corning Q7-2587) USP 0.11 Sucrose - Ultrafine Granules EP / NF 23.04 polyethylene glycol 3350 NF / EP 1.08 polyethylene glycol 400 NF / EP 0.54 Polysorbate 80 NF / EP, JP 0.65 Microcrystalline Cellulose Balls, Grade: CP-305 NF / EP 16.65 total 100.0
[0551] Table 5 summarizes the function of the ingredients used in th...
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