Preparation device of dispersed-phase emulsified oil with ultrafine particle size
A preparation device and ultra-fine technology, used in transportation and packaging, chemical instruments and methods, chemical/physical processes, etc., can solve the problems of large particle size of dispersed phase, difficult to remove, and affect the content of dispersed phase components of emulsified oil. Accuracy and other issues, to achieve uniform particle size of the dispersed phase and reduce the particle size of the dispersed phase
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[0031] A preparation device for preparing dispersed phase ultra-fine particle size emulsified oil comprises an emulsification tank, an ultrasonic emulsification mechanism, a stirring mechanism, a sliding mechanism and a temperature control mechanism.
[0032] like figure 1shown, wherein the emulsification tank includes a semicircular tank cover 1 and a tank body 4, a tangential liquid injection port 2 is opened above the semicircular tank cover 4, and a stirring motor support base 3 is arranged in the center; There is a female rotary LTR type ball spline 301 and a sealing ring 302; one side of the tank body 4 is provided with a connected liquid level gauge 5 to observe the height of the emulsion in the tank, which can be used as a reference for setting the displacement range of the slider 16. A liquid outlet 7 is set on the side to collect the emulsion and discharge the waste liquid, and the bottom is provided with an inclined iron plate baffle 8 inclined at 3 to 5° to ensure ...
Embodiment 1
[0054] Span-80 and Op-10 were used as dispersed phase water ultra-fine particle emulsified diesel composite surfactants, and the optimum hydrophilic-lipophilic balance HLB was 5-6. The HLB of Span-80 is 4.5, the HLB of Op-10 is 14.5, and the mass ratio of Span-80 and Op-10 is 11.5:1. The emulsified diesel oil was prepared from the following raw materials in parts by weight: 87.8 parts of diesel oil, 9.8 parts of deionized water, 2.2 parts of Span-80, and 0.2 parts of Op-10.
[0055] The preparation method of a certain emulsified oil dispersed phase water ultra-fine particle emulsified diesel oil is as follows:
[0056] Add 87.8 parts diesel, 2.2 parts Span-80 to a beaker and stir until the solution becomes clear; then add 9.8 parts deionized water and 0.2 parts Op-10 to another beaker and stir until the solution is clear. Pour it into the emulsification tank from the tangential injection port.
[0057] The emulsification temperature is set to 20-35℃, and the speed of the sti...
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