Concrete segregation repairing agent and preparation method thereof
A concrete and repair agent technology, applied in the field of building materials, can solve the problems affecting the fluidity and strength of concrete, and achieve the effect of not affecting the pumping performance, good viscoelasticity, and good compatibility
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Embodiment 1
[0018] A preparation method for concrete segregation repairing agent, comprising the following steps:
[0019] Step 1. Mixing: Weigh 80 parts of deionized water, 19 parts of 2-acrylamide-2-methylpropanesulfonic acid, 5 parts of acrylic acid, 3 parts of fumaric acid, and 19 parts of acrylamide crystals, and put them into the reaction kettle in turn , stir evenly to obtain a mixture;
[0020] Step 2, neutralization: adding sodium hydroxide solution to the reaction kettle, neutralizing the mixture obtained in step 1 to a pH of 5.5 to 7.0 to obtain a neutralized product;
[0021] Step 3, Polymerization: Warm up the neutralized product obtained in Step 2 to 68-72°C, under the protection of nitrogen, add 0.05 parts of potassium persulfate solution prepared by potassium persulfate at one time, initiate polymerization, and obtain a polymerization product ;
[0022] Step 4. Cool down: when the temperature rises to 95-100°C, add 20 parts of deionized water to the polymerization produc...
Embodiment 2
[0025] A preparation method for concrete segregation repairing agent, comprising the following steps:
[0026] Step 1. Mixing: Weigh 90 parts of deionized water, 15 parts of 2-acrylamide-2-methylpropanesulfonic acid, 4 parts of acrylic acid, 2 parts of fumaric acid, and 17 parts of acrylamide crystals, and put them into the reaction kettle in turn , stir evenly to obtain a mixture;
[0027] Step 2, neutralization: adding sodium hydroxide solution to the reaction kettle, neutralizing the mixture obtained in step 1 to a pH of 5.5 to 7.0 to obtain a neutralized product;
[0028] Step 3, Polymerization: Warm up the neutralized product obtained in Step 2 to 68-72°C, under the protection of nitrogen, add 0.03 parts of potassium persulfate solution prepared by potassium persulfate at one time, initiate polymerization, and obtain a polymerization product ;
[0029] Step 4. Cool down: when the temperature rises to 95-100°C, add 20 parts of deionized water to the polymerization produc...
Embodiment 3
[0032] A preparation method for concrete segregation repairing agent, comprising the following steps:
[0033] Step 1. Mixing: Weigh 100 parts of deionized water, 11 parts of 2-acrylamide-2-methylpropanesulfonic acid, 3 parts of acrylic acid, 1 part of fumaric acid, and 16 parts of acrylamide crystals, and put them into the reaction kettle in turn , stir evenly to obtain a mixture;
[0034] Step 2, neutralization: adding sodium hydroxide solution to the reaction kettle, neutralizing the mixture obtained in step 1 to a pH of 5.5 to 7.0 to obtain a neutralized product;
[0035] Step 3, Polymerization: Warm up the neutralized product obtained in Step 2 to 68-72°C, under the protection of nitrogen, add 0.02 parts of potassium persulfate solution prepared by potassium persulfate at one time, initiate polymerization, and obtain a polymerization product ;
[0036] Step 4. Cool down: when the temperature rises to 95-100°C, add 20 parts of deionized water to the polymerization produc...
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