Light excitation and cell iron death combined induced bionic drug carrier as well as preparation method and application thereof
A technology of ferroptosis and photoexcitation, which is applied in the direction of drug combinations, pharmaceutical formulations, medical preparations of non-active ingredients, etc., can solve the problem of uneven distribution of dihydroartemisinin tumor sites, achieve good aqueous solution dispersion, and improve utilization rate, the effect of increasing the ferroptosis induction effect
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Embodiment 1
[0055] Embodiment 1: Preparation of CM / DHA@ZIF-90-Fe-TA
[0056] (1) Dissolve 10 mg of dihydroartemisinin in 2 ml of N, N-dimethylformamide and 43.8 mg of zinc acetate in 2 ml of N, N-dimethylformamide, mix them, stir at room temperature for 2 hours, use The zinc ion of zinc acetate and dihydroartemisinin form a coordination bond;
[0057] (2) Dissolve 38.6mg of 2-imidazole formaldehyde in 2ml of N,N-dimethylformamide and stir at 70°C until completely dissolved;
[0058] (3) Mix the above two solutions, stir and react for 5 minutes, add 10ml N, N-dimethylformamide to it, continue stirring for 20 minutes, centrifuge at 12000rmp for 15 minutes, and then use N, N-dimethylformamide respectively Dimethyl formamide and ethanol were washed three times to remove unreacted reagents, and dried at room temperature to obtain DHA@ZIF-90 carrier;
[0059] (4) 50 mg of tannic acid is dissolved into 5 ml of deionized water;
[0060] (5) Add 100mg of DHA@ZIF-90 carrier, ultrasonically oscil...
Embodiment 2
[0063] Embodiment 2: Preparation of CM / DHA@ZIF-90-Fe-TA
[0064] (1) Dissolve 50 mg of dihydroartemisinin in 4 ml of N, N-dimethylformamide and 43.8 mg of zinc acetate dissolved in 2 ml of N, N-dimethylformamide, mix them, stir at room temperature for 2 hours, use The zinc ion of zinc acetate and dihydroartemisinin form a coordination bond;
[0065] (2) Dissolve 200mg of 2-imidazole formaldehyde in 100ml of N,N-dimethylformamide and stir at 70°C until completely dissolved;
[0066] (3) Mix the above two solutions, stir and react for 10 minutes, add 10ml N, N-dimethylformamide to it, continue stirring for 20 minutes, centrifuge at 12000rmp for 15 minutes, and then use N, N-dimethylformamide respectively Dimethyl formamide and ethanol were washed three times to remove unreacted reagents, and dried at room temperature to obtain DHA@ZIF-90 carrier;
[0067] (4) 100mg of tannic acid is dissolved in 5ml of deionized water;
[0068] (5) Add 100mg of DHA@ZIF-90 carrier, ultrasonica...
Embodiment 3
[0071] Embodiment 3: Preparation of CM / DHA@ZIF-90-Fe-TA
[0072] (1) Dissolve 200mg of dihydroartemisinin in 10ml of N,N-dimethylformamide and 300mg of zinc acetate in 10ml of N,N-dimethylformamide solution, stir at room temperature for 2h, and use acetic acid The zinc ion of zinc and dihydroartemisinin form a coordination bond;
[0073] (2) Dissolve 200mg of 2-imidazole formaldehyde in 10ml of N,N-dimethylformamide, and stir at 70°C until completely dissolved;
[0074] (3) Mix the above two solutions, stir and react for 5 minutes, add 10ml N, N-dimethylformamide to it, continue stirring for 20 minutes, centrifuge at 12000rmp for 15 minutes, and then use N, N-dimethylformamide Dimethyl formamide and ethanol were washed three times to remove unreacted reagents, and dried at room temperature to obtain DHA@ZIF-90 carrier;
[0075] (4) 200mg of tannic acid is dissolved into 5ml of deionized water;
[0076] (5) Add 100mg of DHA@ZIF-90 carrier, ultrasonically oscillate evenly, an...
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