Novel high-temperature-resistant epoxy resin adhesive as well as preparation method and use method thereof

An epoxy resin glue, epoxy resin technology, applied in the direction of epoxy resin glue, bonding method, adhesive, etc., can solve the problems of air bubbles, poor fluidity of epoxy glue, insufficient filling, etc., to achieve broad application prospects, Excellent insulation performance

Pending Publication Date: 2021-03-16
SHAANXI HUADA SCI TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The existing epoxy adhesives cannot meet the actual use requirements when potting RF connectors. There is an urgent need for high temperature resistant potting RF connectors. According to the survey results, it is known that the potting adhesives currently used in RF connectors in the industry are mainly It is E44, E-51 epoxy glue system, the epoxy glue of this system is not resistant to high temperature, and when it is stirred unevenly, there will be bubbles, and there will be unqualified insulation resistance.
In addition, the ambient temperature and humidity during potting have a great influence on the potting quality of the product. In a low temperature environment, the fluidity of epoxy glue is poor. During the mixing process, air bubbles are likely to be generated, and it is easy to cause insufficient filling during potting. , and in a higher temperature environment, the epoxy glue has a greater fluidity, and it is easy to produce glue outflow during potting

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] In this example, the new high-temperature-resistant epoxy resin glue includes the following substances in parts by mass: 8-12 parts of epoxy resin; 0.9-1.3 parts of aromatic amine-based high-temperature-resistant curing agent; and 3-4 parts of epoxy curing agent.

[0025] It should be noted that the epoxy resin is one of E51 epoxy resin or CYD-128 epoxy resin, and the high temperature resistant curing agent is aromatic amine high temperature resistant curing agent, SH-200 high temperature toughening curing agent or BD One of the epoxy curing agents, the epoxy curing agent is one of the R-2023 epoxy curing agent or the R-2285 epoxy curing agent.

Embodiment 2

[0027] In this example, the new high-temperature-resistant epoxy resin glue includes the following substances in parts by mass: 9-11 parts of epoxy resin; 1-1.2 parts of aromatic amine high-temperature-resistant curing agent; 3.2-3.4 parts of epoxy curing agent.

[0028] It should be noted that the epoxy resin is one of E51 type epoxy resin or CYD-128 type epoxy resin, and the epoxy resin is preferably E51 type epoxy resin. The high temperature resistant curing agent is one of aromatic amine high temperature resistant curing agent, SH-200 high temperature toughening curing agent or BD type curing agent, and the high temperature resistant curing agent is preferably BD type curing agent. Epoxy curing agent is a kind of in R-2023 type epoxy curing agent or R-2285 type epoxy curing agent, and epoxy curing agent is preferred R-2285 type epoxy curing agent.

[0029] Specifically, R-2023 epoxy curing agent: the drying time of the film is 10 minutes at room temperature 25°C, the ratio...

Embodiment 3

[0031] In this embodiment, the preparation method of the novel high temperature resistant epoxy resin glue comprises the following preparation steps:

[0032] 1) Fully stir and mix 8-12 parts by mass of epoxy resin, 0.9-1.3 parts by mass of aromatic amine high-temperature-resistant curing agent, and 3-4 parts by mass of epoxy curing agent to obtain the initial potting glue;

[0033] 2) Perform defoaming treatment on the uniformly mixed initial potting compound to obtain the defoaming potting compound;

[0034] 3) After the defoaming potting compound is left to stand, the finished potting compound is obtained.

[0035] It should be noted that the stirring, mixing and defoaming steps can be performed using existing equipment.

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Abstract

The invention discloses a novel high-temperature-resistant epoxy resin adhesive as well as a preparation method and a use method thereof, and relates to the technical field of novel adhesives, the novel high-temperature-resistant epoxy resin adhesive comprises the following substances in parts by mass: 8-12 parts of epoxy resin, 0.9-1.3 parts of aromatic amine high-temperature-resistant curing agent and 3-4 parts of epoxy curing agent, by adopting the processes of novel configuration, centrifugal defoaming, glue filling and the like, the produced epoxy resin glue has the advantages of high temperature resistance and no bubbles, and compared with the prior art, the patent of the invention adopts novel raw materials, a novel ratio and a novel process, tests show that the insulating propertyis excellent under different humidity and temperature, and the condition that the insulating resistance is reduced does not occur; the requirements of dielectric voltage resistance and insulation resistance of products can be met, and the application prospect is wide.

Description

technical field [0001] The invention relates to the technical field of novel adhesives, in particular to a novel high-temperature-resistant epoxy resin adhesive and a method for making and using the same. Background technique [0002] Epoxy adhesive is a liquid or solid adhesive composed of epoxy resin, curing agent, accelerator, modifier, etc. Since epoxy resin contains a variety of polar groups and highly active epoxy groups, it has strong adhesion to various polar materials such as metal, glass, cement, wood, plastics, etc. The cohesive strength is also very large, so the bonding strength is very high. Epoxy resin adhesives have been widely used in industry and life because of their excellent comprehensive properties. The development of modern science and technology such as automobiles and electronics has put forward higher requirements for the temperature resistance of adhesives. [0003] The existing epoxy adhesives cannot meet the actual use requirements when pottin...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09J163/00C09J5/00C08G59/50C08G59/56
CPCC09J163/00C09J5/00C08G59/5033C08G59/56
Inventor 郭嬿戴世慧武婷
Owner SHAANXI HUADA SCI TECH
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