Modified bamboo biochar material for treating cadmium pollution in water and preparation method of modified bamboo biochar material
A biochar, cadmium pollution technology, applied in water pollutants, chemical instruments and methods, other chemical processes, etc., can solve the problems of easy analysis, small adsorption capacity, etc., to improve production efficiency, short process flow, and improve active functional groups. Effect
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Embodiment 1
[0024] The materials and reagents used in this example can be obtained from commercial sources unless otherwise specified.
[0025] The bamboo stalks in this embodiment are preferably mature bamboo, or its processing residues. The mature bamboo stalks are chopped into chunky fragments with a length and width below 1 cm, divided into six parts, then dried at 100 ± 5 ° C, and then dried in a vacuum Carbonization treatment in the state: vacuum degree is about 0.068MPa, first heat to 90°C, keep for 30min, then heat from 90°C to 300°C, keep for 1h to complete carbonization. Six parts of charred bamboo were activated at 500, 600, 700, 800, 900 and 1000 °C for 2 h, and at the same time, when heating from 300 °C, all of them were filled with N 2 The gas is protected, and the N2 flow rate is maintained at 30-45ml / min. The yields of bamboo biochar are: 16.94, 15.02, 14.14, 14.13, 13.95, and 13.86. It can be seen that with the increase of activation temperature, the charcoal yield Gradu...
Embodiment 2
[0036] The difference between Example 2 and Example 1 is that Nanzhu is replaced by adult cotton bamboo as the preparation material. Through the same preparation steps and adsorption experiments as in Example 1, it is found that there is no significant difference in the adsorption effect. The results are shown in image 3 .
Embodiment 3
[0038] Considering the cost factor, the difference from Example 1 is that the carbonization and activation stages are not charged with N 2 Gas, the research results show that the carbon yield of bamboo biochar tends to decrease. Under the same preparation temperature, the char yield decreases by about 6%, and the adsorption rate of modified bamboo biochar decreases slightly. The adsorption rate of cadmium under the same conditions rate decreased by 1.3 to 4.2%.
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