Low-temperature battery electrolytic solution based on ionic liquid, preparation method and application thereof
An ionic liquid, low-temperature lithium battery technology, applied in the field of lithium-ion battery electrolyte materials, can solve the problems of unfavorable battery capacity, high cost, high low-temperature viscosity of ionic liquid, etc. Effect
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Embodiment 1
[0027] This embodiment provides a low-temperature lithium battery electrolyte based on ionic liquid and its preparation method, specifically:
[0028] (a) Under argon protection, measure 1.0 mL of 1-ethyl-3-methylimidazole bistrifluoromethanesulfonimide ionic liquid in a glove box, and then weigh 0.374 g of bis(fluorosulfonyl Acyl) imide lithium (LiFSA), stir evenly, the amount concentration of LiFSA in this ionic liquid electrolyte is 2.0M;
[0029] (b) Add 1.0 mL of anhydrous dichloromethane to the above electrolytic solution; after fully mixing, the low-temperature electrolytic solution is obtained; the lithium salt concentration in the electrolytic solution is 1.0M.
Embodiment 2
[0031] This embodiment provides an ionic liquid-based low-temperature lithium battery electrolyte and its configuration method, specifically:
[0032] (a) Under argon protection, measure 1.0 mL of N-butyl-N-methylpyrrolidine bistrifluoromethanesulfonimide salt ionic liquid in a glove box, and then weigh 0.574 g of bistrifluoromethanesulfonimide ionic liquid Lithium methanesulfonylimide (LiTFSI), stirred evenly, the concentration of LiTFSI in the ionic liquid electrolyte is 2.0M;
[0033] (b) Add 4.0 mL of anhydrous dichloromethane to the above electrolytic solution; after fully mixing, the low-temperature electrolytic solution is obtained; the lithium salt concentration in the electrolytic solution is 0.4M.
Embodiment 3
[0035] This embodiment provides an ionic liquid-based low-temperature lithium battery electrolyte and its configuration method, specifically:
[0036] (a) Under argon protection, measure 1.0 mL of N-butyl-N-methylpyrrolidine bistrifluoromethanesulfonimide salt ionic liquid in a glove box, and then weigh 0.152 g of lithium hexafluorophosphate ( LiPF 6 ) mixed evenly, the LiPF in the ionic liquid electrolyte 6 The concentration of the substance is 1.0M;
[0037] (b) After mixing evenly, add 1.0mL of 1,1,2,2-tetrafluoroethyl-2,2,2-trifluoroethyl ether to the above electrolytic solution; low-temperature electrolyte; in this electrolyte, the lithium salt concentration is 0.5M.
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