Settling separation method for nickel leaching solution

A technology of sedimentation separation and leaching liquid, applied in the direction of improving process efficiency, can solve the problems such as the decline of extraction production capacity, the increase of the third phase in the extraction process, the increase of production costs, etc., to prevent the loss of valuable metal materials, reduce production costs, The effect of increasing production capacity

Inactive Publication Date: 2021-07-09
JINCHUAN GROUP LIMITED
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Due to the particularity of raw materials in the production process, the difficulty of end-point control and other factors, the leaching thickener often has poor settling effect and the overflow liquid of the thickener "runs muddy", which not only leads to the failure rate of the precision filter of the leachate High, the liquid after filtration is not clear, which will lead to the increase of the third phase in the extraction process, and the failure rate of extraction and stripping equipment will increase, thereby reducing the extraction production capacity, which will eventually lead to problems such as production capacity not meeting the design requirements and increased production costs.

Method used

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  • Settling separation method for nickel leaching solution
  • Settling separation method for nickel leaching solution

Examples

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Effect test

Embodiment 1

[0023] Laboratory flocculation sedimentation test, process flow see attached figure 1 .

[0024] Take a 200L section of normal pressure leaching thickener overflow liquid for laboratory flocculation and sedimentation test. The test was carried out in a mud bucket with a height of 1.4m and a diameter of 0.35m. A peristaltic pump was used to continuously feed (overflow liquid), the feeding rate was 1L / min, the flow rate of 1‰ flocculant was 6mL / min, and the flocculation and sedimentation supernatant was collected continuously. Filter the flocculation supernatant with a vacuum filter. The filtered solution was subjected to extraction test. Test results: The solid content of the flocculation supernatant is 0.35g / L (about 0.026%), and the solid content is reduced by 94.60% compared with the overflow liquid of the on-site thickener (the on-site solid content is 6.5-7.0g / L). After the flocculation supernatant is filtered The liquid is clear and free of particles. The extraction ...

Embodiment 2

[0026] On-site industrial small-scale test, the process flow is attached figure 2 .

[0027] Using the existing equipment on site to carry out transformation, part of a section of normal pressure leachate overflow (5m 3 / h) into 10m through the pipe 3 In the normal pressure intermediate tank, at the same time, add PAM-800 flocculant into the dissolution tank at a rate of 30g / h, and open the air duct and heating return pipe to dissolve the flocculant. After the dissolution is complete, open the valve and inject the flocculant into 10m 3 In the normal pressure intermediate tank, the flocculation reaction time is 5 to 10 minutes. Then pump in 6m through the solution transfer pump 3 Dense sedimentation separation is carried out in the clarification separation tank. The supernatant was returned to 300m 2 The precision filter is filtered, and the flocculation bottom flow is returned to the normal pressure liquid slurry tank. After 20 minutes of sedimentation and clarificatio...

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Abstract

The invention discloses a settling separation method for a nickel leaching solution, and relates to an improvement of the settling separation method for the nickel leaching solution in the process of producing metallic nickel by adopting hydrometallurgy. The separation process comprises the following steps of carrying out dense separation on ore pulp produced in a leaching process by adopting a thickener, and filtering dense overflow supernate by adopting a precision machine; and the method is characterized by further comprising the following steps of adding a flocculating agent into the overflow supernate which is subjected to dense separation by adopting the thickener for a flocculating settling reaction, and carrying out precise separation on the supernate which is subjected to flocculating settling. According to the method, the chemical property of the overflow liquid is not changed, the content of main valuable elements is basically unchanged, only the solid content in the overflow liquid is agglomerated, the sedimentation of the solid content is accelerated, the effect is good, the loss of valuable metal materials in the thickening process is effectively prevented, and the production cost is reduced.

Description

technical field [0001] The invention discloses a method for sedimentation and separation of nickel leaching solution, which relates to an improvement of the method for sedimentation and separation of nickel leaching solution in the process of producing metal nickel by hydrometallurgy. Background technique [0002] In the process of wet production of metallic nickel, the production process includes the process steps of "leaching-extraction-electrodeposition" to produce electrolytic nickel. Among them, the ore pulp produced in the leaching process is first thickened and separated by a thickener, and the thick overflow supernatant is filtered by a precision machine to make the leachate meet the requirements of subsequent extraction production. [0003] Due to the particularity of raw materials in the production process, the difficulty of end-point control and other factors, the leaching thickener often has poor settling effect and the overflow liquid of the thickener "runs mudd...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22B3/22C22B23/00
CPCC22B3/22C22B23/0453Y02P10/20
Inventor 马磊周通陈涛李瑞基闫刚刚程应峰张雯雯张文生李瑞杰曹勇虎桂芳卫媛
Owner JINCHUAN GROUP LIMITED
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