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Rubber final mixing process for internal mixer

An internal mixer and rubber technology, used in the field of rubber mixing, can solve the problems of increased energy consumption, high energy consumption, and short rubber compound mixing time, so as to reduce the impact of equipment, the principle is scientific and reliable, and the final mixing energy can be reduced. consumption effect

Active Publication Date: 2021-07-27
QINGDAO UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Most final mixing internal mixers use low speed to prevent rapid temperature rise, but the shearing and kneading action of the rotor of the internal mixer will still produce a large temperature rise, and will make the masterbatched rubber produce more Shearing breaks the chain, affecting the performance of the compound
At the same time, the faster temperature rise will also lead to short mixing time of rubber materials, uneven mixing time between different batches, large differences in final rubber vulcanization curves, low production efficiency, and difficulty in meeting production needs
[0004] In addition, when the rubber industry conducts final refining with internal mixers, it will try to reduce the final refining temperature to prevent scorching. However, during the final refining process , the lower temperature of the mixed rubber will heat up rapidly under the shearing and kneading action of the rotor; when the interval between the two stages of mixing is long, the mixed rubber will become hard, and if the internal mixer is directly added to the final mixing Hard rubber compound will have a greater impact on the internal mixer, resulting in a large torque mutation, loss of equipment, and increased energy consumption
If the mixed rubber is heated up, pressed into tablets or crushed and added to the internal mixer, the steps are complicated and the energy consumption is high

Method used

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  • Rubber final mixing process for internal mixer
  • Rubber final mixing process for internal mixer
  • Rubber final mixing process for internal mixer

Examples

Experimental program
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Effect test

Embodiment 1

[0019] The concrete steps of the rubber final mixing process used in the internal mixer involved in the present embodiment are:

[0020] (1) Raise the temperature of the mixing chamber with a capacity of 200 mL of the RM-200C internal mixer (using Erleng Bunbury rotor) of Harbin Hapu Electric Technology Co., Ltd. to 120 °C and wait for use;

[0021] (2) Add the sulfur into the mixing chamber with a rotating speed of 10 rpm, and drop the top bolt to keep the temperature for 30s, so that all the sulfur is transformed into a molten state; when adding sulfur, avoid the sulfur falling on the rotor, and try to let the sulfur fall on the wall of the mixing chamber. , to avoid slippage between the rotor and the rubber material, reduce the friction coefficient between the mixing chamber wall and the rubber material, and increase the feeding speed; avoid open flames and static electricity, and do not use high speed before the sulfur is melted, in order to prevent safety problems caused b...

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PUM

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Abstract

The invention belongs to the technical field of rubber mixing, and relates to a rubber final mixing process for an internal mixer. The rubber final mixing process comprises the following specific steps that (1) the temperature of an internal mixing chamber is increased to 120 DEG C; (2) a vulcanizing agent is added into the internal mixing chamber, and a top peg is dropped down for heat preservation; (3) chopped mixed rubber blocks are added into the internal mixing chamber; and (4) an accelerant is immediately added after the mixed rubber blocks are added, the top peg is dropped down for mixing, the temperature of the internal mixing chamber is set to be higher, the Mooney viscosity of rubber materials is quickly reduced under the action of liquid sulfur, the shearing action of a rotor is reduced, the temperature of the whole internal mixing chamber is reduced by rubber compound with lower temperature, and the temperature is kept within a proper range. The vulcanizing agent is firstly added for melting, then the rubber compound is added, the rubber compound is uniformly mixed with the vulcanizing agent in the heating plastication process, the accelerant is immediately added for mixing after rubber adding, the vulcanizing agent and the accelerant are separately added, and the accelerant is added at the last, so that the scorching phenomenon of the rubber materials can be avoided to the greatest extent.

Description

Technical field: [0001] The invention belongs to the technical field of rubber mixing, and relates to a rubber final mixing process for an internal mixer, which can improve production efficiency. Background technique: [0002] Final mixing is an indispensable and important step in the rubber processing process: adding vulcanizing agent and accelerator to the rubber compound after mixing in the internal mixer or open mixer, and mixing it evenly, it is unloaded. The vulcanizing agent is mainly sulfur. The melting point of industrial sulfur is 112.8 °C and the flash point is 207 °C. The ordinary rubber processing will not reach the flash point of sulfur. Controlling static electricity and open flames during processing can ensure processing safety. The addition of sulfur can reduce the Mooney viscosity of the rubber compound, and a higher mixing temperature can also reduce the Mooney viscosity of the rubber compound and improve the processability. [0003] The traditional final...

Claims

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Application Information

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IPC IPC(8): B29B7/00
CPCB29B7/005B29B7/7495B29B7/826B29B7/823B29B7/286B29B7/183
Inventor 边慧光肖鑫鑫王禄银许明辉汪传生王志飞
Owner QINGDAO UNIV OF SCI & TECH
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