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152results about "Working-up pitch/asphalt/bitumen by solidifying/disintegrating" patented technology

Deep separation method and processing system for the separation of heavy oil through granulation of coupled post-extraction asphalt residue

The present invention is a separation method and system in which granulation of coupled post-extraction asphalt residue is used to achieve deep separation of heavy oil. A dispersion solvent is introduced into the asphalt phase after separation by solvent extraction and the asphalt phase undergoes rapid phase change in a gas-solid separator and is dispersed into solid particles while the solvent vaporizes, resulting in low temperature separation of asphalt and solvent with adjustable size of the asphalt particles. The separation method of this invention also includes a three-stage separation of heavy oil feedstock, in which the deasphalted oil phase separated from heavy oil is treated with supercritical solvent and results in the further separation of the resin portion of the deasphalted oil, maximizing the yield and quality of the deasphalted oil. The processes and systems in this invention use atmospheric pressure and a low temperature gas-solid separator instead of a high temperature and high pressure furnace and do not require the feed pre-heating or heat exchange equipment at the inlet of resin separator column, resulting in a simplified process flow and reduced investment.
Owner:CHINA UNIV OF PETROLEUM (BEIJING)

Deep separation method and processing system for the separation of heavy oil through granulation of coupled post-extraction asphalt residue

The present invention is a separation method and system in which granulation of coupled post-extraction asphalt residue is used to achieve deep separation of heavy oil. A dispersion solvent is introduced into the asphalt phase after separation by solvent extraction and the asphalt phase undergoes rapid phase change in a gas-solid separator and is dispersed into solid particles while the solvent vaporizes, resulting in low temperature separation of asphalt and solvent with adjustable size of the asphalt particles. The separation method of this invention also includes a three-stage separation of heavy oil feedstock, in which the deasphalted oil phase separated from heavy oil is treated with supercritical solvent and results in the further separation of the resin portion of the deasphalted oil, maximizing the yield and quality of the deasphalted oil. The processes and systems in this invention use atmospheric pressure and a low temperature gas-solid separator instead of a high temperature and high pressure furnace and do not require the feed pre-heating or heat exchange equipment at the inlet of resin separator column, resulting in a simplified process flow and reduced investment.
Owner:CHINA UNIV OF PETROLEUM (BEIJING)

High-softening-point asphalt as well as preparation method and application thereof

The invention discloses a high-softening-point asphalt as well as a preparation method and an application thereof. Medium-temperature asphalt is adopted as a raw material to prepare high-softening-point asphalt by adopting an air oxidation method; then partial light components in the high-softening-point asphalt are removed by adopting a vacuumizing method, and finally the high-softening-point asphalt suitable for preparing foam carbon or spinning asphalt can be produced. The softening point of the high-softening-point asphalt is 200 to 280 DEG C, the content of an n-heptane soluble substance (HS) is less than 10 percent, the content of a methylbenzene soluble substance (TS) is less than 20 percent, the content of methylbenzene insoluble-pyridine soluble sustancce (TI-PS) is 9 to 20 percent, the content of pyridine insoluble-quinoline soluble (PI-QS) is 5 to 15 percent, and the content of quinoline insoluble substance (QI) I 50 to 70 percent. The high-softening-point asphalt is not only rich in raw materials and low in cost, but also narrow in group composition distribution and suitable for being used as a raw material for high-performance foam carbon and carbon fibers.
Owner:BAOWU CHARCOAL MATERIAL TECH CO LTD +1

Asphalt crushing and melting equipment for municipal construction

The invention discloses an asphalt crushing and melting equipment for municipal construction, which comprises a non-melting slag discharge pipe, a heating sleeve, a grinding roller, a fixed breaking hammer and an asphalt melting tank. A support frame is installed at the bottom of the asphalt melting tank. The upper end of the melting tank is connected to the asphalt input pipe; the top of the asphalt melting tank is equipped with a stirring motor, the rotating shaft of the stirring motor is connected to the rotating shaft through a coupling, and the rotating shaft is installed vertically inside the asphalt melting tank, and the top of the rotating shaft is welded Breaker, the bottom side of the rotary breaker is equipped with a number of rotating breaker teeth, and the bottom side of the rotary breaker is equipped with a fixed breaker; it realizes the convenient addition of asphalt blocks and avoids clogging; it realizes grinding treatment and further crushing, which is convenient for asphalt Block melting operation; realize the separate discharge of non-melting slag and asphalt melt, improve the effect and quality of asphalt melting; it is beneficial to the melting of asphalt, the heat transfer oil circulates, and the heating effect is good.
Owner:CHANGSHA KEYUE ENTERPRISE MANAGEMENT CONSULTING CO LTD

Preparation method of bitumen balls

The invention discloses a preparation method of bitumen balls, which comprises the following steps: 1) putting viscosity depressants into a reaction kettle, heating and melting; under the condition of stirring, adding bitumen with high softening point; under the condition of stirring, heating the reaction kettle to a temperature not lower than the softening point of the bitumen with the high softening point and keeping the temperature for 1-3 hours; and cooling to obtain the prepared bitumen, wherein the softening point of the bitumen with high softening point is 180-300 DEG C; and 2) heating the prepared bitumen to 90-180DEG C, and enabling the bitumen has mobility, in the state of heat preservation, adding the prepared bitumen below the suspending medium liquid level of which the temperature is 80-90 DEG C, keeping for 1-10min at the temperature of 80-90 DEG C, and cooling to obtain the bitumen balls, wherein the suspending medium is polyving alcohol aqueous solution. The method of the invention has the characteristics of full utilization of raw materials of bitumen, reduced waste of raw materials, simple preparation process, and low production cost; and the bitumen ball prepared by the method is more uniform, and has smoother surface, thus avoiding the crash and adhesion of bitumen balls.
Owner:CHINA NAT OFFSHORE OIL CORP +1

Spraying and granulating separation column with jacket cooling system on taper section

The invention relates to a spraying and granulating separation column with a jacket cooling system on a taper section. The main structure of the separation column mainly comprises a granulating column body, a spraying and granulating nozzle system and a lower discharge pot from top to bottom, wherein the granulating column body can be formed by a separation and precipitation section, a taper section and a jacket cooling system; the spraying and granulating nozzle system can be formed by a distributor master pipe and a plurality of distributor branch pipes; the distributor branch pipes are symmetrically distributed, and the jet direction of the outlets of the distributor branch pipes form a certain angle with the vertical direction, which can form a rotating flow field with tangential velocity; the jacket cooling system comprises a tangential cooling water outlet, a radial cooling water inlet and a jacket main body; and cooling water rotates and upwards flows in a jacket, separated particles rotate and downwards flow in the spraying and granulating separation column, and the rotating and flowing directions of the cooling water and the separated particles are opposite to form contranatant heat exchange. In the invention, rotating flow fields of different degrees can be formed in the granulating column through adjusting the angles of the charge distributor and the number of the distributor branch pipes to realize different particle distribution states and improve the gas-solid separation efficiency; and different heat exchange efficiencies can be realized through adjusting the temperature, the pressure and the flow rate of a cooling water inlet and the structural size of a cooling water jack, and then the particle temperature can be reduced to control the temperature of the granulating column.
Owner:CHINA UNIV OF PETROLEUM (BEIJING)

Pouring steel belt type asphalt granulation production unit

The embodiment of the invention discloses a pouring steel belt type asphalt granulation production unit. The pouring steel belt type asphalt granulation production unit comprises a material heat-preservation system, a lifting-moving pouring granulation system, a cooling and conveying system and a finished product packaging system, wherein the material heat-preservation system is connected with thelifting-moving pouring granulation system through a feeding pipeline and used for preserving asphalt for a shell and asphalt for an inner core and delivering the asphalt for the shell and the asphaltfor the inner core to the lifting-moving pouring granulation system through the feeding pipeline and a material pump; the lifting-moving pouring granulation system is used for pouring granulation ofthe asphalt for the shell and the asphalt for the inner core and forming liquid granules to be output; the cooling and conveying system is connected with the lifting-moving pouring granulation systemand used for cooling the liquid granules output by the lifting-moving pouring granulation system to form solid granular asphalt to be output; and the finished product packaging system is connected with the cooling and conveying system and used for packaging the solid granular asphalt output by the cooling and conveying system. The pouring steel belt type asphalt granulation production unit has thecharacteristics of easy operation, continuous production, high automation degree and high production efficiency.
Owner:北京紫瑞天成科技有限公司

Apparatus and method for recovering solvent in granulation of de-oiled asphalt with high softening point

The invention relates to an apparatus and a method for recovering a solvent in granulation of de-oiled asphalt with a high softening point. Specifically speaking, the de-oiled asphalt with a high softening point discharged from the bottom of a solvent deasphalting tower is granulated through a screw extrusion system, and obtained granular de-oiled asphalt is directly introduced into a de-oiled asphalt solvent enrichment chamber; and the top of the solvent enrichment chamber is provided with a solvent gas recovery pipeline communicated with a solvent recovery system, and facilities like a de-oiled asphalt solid particle water entering slideway are arranged in the chamber so as to prevent the de-oiled asphalt from directly falling into cooling water and prolonging time for releasing of the solvent by the granular de-oiled asphalt. Compared to the prior art, the method for recovering the solvent in granulation of the de-oiled asphalt with a high softening point has the following advantages: the whole process is simple and easily practicable, equipment like a heating furnace and a stripping tower in a conventional de-oiled asphalt solvent separation unit are omitted, and the phenomena of high energy consumption, long flow process and instable operation in recovery of the solvent used for the de-oiled asphalt with a high softening point are avoided.
Owner:CHINA PETROLEUM & CHEM CORP +1

Coal pitch refining method used for synthesizing mesophase pitch

The invention relates to a coal pitch refining method used for synthesizing mesophase pitch. The coal pitch refining method used for synthesizing mesophase pitch comprises following steps: coal pitchis smashed and sieved, a mixed solvent A is added into coal pitch, an obtained mixture is stirred, is allowed to stand, and is subjected to layering so as to obtain an upper layer which is a mixed solution A of the mixed solvent A and coal pitch, and a lower layer which is an impurity mixture containing coal powder coke particles; the upper layer mixed solution A is subjected to filtering and distillation for recovery of the mixed solvent A so as to obtain crude coal pitch; a mixed solvent B is added into the crude coal pitch, and stirring, standing, and layering are carried out so as to obtain an upper layer which is a mixed solution B of the mixed solvent B and refined coal pitch, and a lower layer which is a heavy asphalt impurity mixture; the upper layer mixed solution B is subjected to filtering and distillation for recovery of the mixed solvent B so as to obtain refined coal pitch can be used for synthesizing mesophase pitch. The coal pitch refining method is capable of realizingseparation of coal pitch effective components with impurities such as coal powder coke particles under normal pressure conditions, the obtained refined coal pitch can be taken as a high grade carbonmaterial raw material, and the requirements of subsequent high added value product production are satisfied.
Owner:SHANDONG RUICHENG AEROSPACE CARBON MATERIAL CO LTD

Purification method for coal pitch with high softening point

The invention discloses a purification method for coal pitch with a high softening point and belongs to the technical field of tar deep processing. The purification method comprises the following steps: mixing pitch with small-molecule aromatic hydrocarbons and obtaining pitch particles by using a granulator and a cutting-off machine; extracting the pitch particles with a solvent to obtain porous pitch particles; extracting the porous tar particles with alkali solution and acid solution to obtain the content of silicon and the content of metal and performing solid-liquid separation; washing the extracted particles with deionized water and performing solid-liquid separation; drying the substances in an inert atmosphere or vacuum environment to obtain purified pitch. The purification method disclosed by the invention has the benefits that the porous pitch particles are extracted by using low-temperature alkali and acid of 30-80DEG C, so that silicon and other metal impurities in the coal pitch are effectively removed; the total ash content of the obtained purified pitch is less than 0.005 percent, the content of the silicon is less than 0.001 percent and the content of the metal impurities is less than 0.002 percent; higher use requirement can be met; besides, the purification method is simple in process step and lower in energy consumption.
Owner:SICHUAN CHUANGYUE CARBON MATERIAL
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