Near-zero expansion coefficient ceramic composite material and preparation method thereof
A ceramic composite material and near-zero expansion technology, applied in the field of ceramic composite materials, can solve the problems of poor dimensional stability, weak bending resistance and toughness, and achieve excellent near-zero expansion performance, good heat resistance effect and high stability. Effect
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[0051] The second aspect of the embodiment of the present application provides a method for preparing a near-zero expansion coefficient ceramic composite material, comprising the following steps:
[0052] S01. Provide each component according to the ceramic composite material with near zero expansion coefficient;
[0053] S02. Performing a first mixing treatment on ceramic raw materials and additives, and performing grinding treatment to obtain a first mixture;
[0054] S03. The first mixture is mixed with hafnium tungstate and Ti-Ni alloy to obtain a second mixture;
[0055] S04. The second mixture is extruded and sintered to obtain a nearly zero expansion coefficient ceramic composite material.
[0056] The preparation method of the near-zero expansion coefficient ceramic composite material provided by the second aspect of the application is simple, the sintering temperature is low, and the preparation cycle is short, which can reduce production costs, save energy consumpti...
Embodiment 1
[0065] A kind of nearly zero expansion coefficient ceramic composite material and preparation method thereof
[0066] A near-zero expansion coefficient ceramic composite material
[0067] Comprising the following components by weight:
[0068]
[0069] Wherein, the ceramic raw material comprises the following components in parts by weight:
[0070] 75 parts of ceramic main material;
[0071] 5 parts of ceramic auxiliary materials; and,
[0072] The main ceramic material is selected from a mixture of zirconia and alumina with an average particle size of 200 nanometers, and the auxiliary ceramic material is selected from silicon nitride with an average particle size of 5 microns;
[0073] Ti-Ni alloys are selected from porous Ti 75 Ni 25 , and the pore size of the porous Ti-Ni alloy is 1 micron;
[0074] Auxiliaries include the following components by weight:
[0075] Filling agent 8 parts;
[0076] Adhesive 0.5 part;
[0077] 0.5 parts of dispersant; and,
[0078]...
Embodiment 2
[0086] A kind of nearly zero expansion coefficient ceramic composite material and preparation method thereof
[0087] A near-zero expansion coefficient ceramic composite material
[0088]Comprising the following components by weight:
[0089]
[0090] Wherein, the ceramic raw material comprises the following components in parts by weight:
[0091] 80 parts of ceramic main material;
[0092] 10 parts of ceramic auxiliary materials; and,
[0093] The main ceramic material is selected from zirconia with an average particle size of 250 nanometers, and the auxiliary ceramic material is selected from silicon nitride with an average particle size of 8 microns;
[0094] Ti-Ni alloys are selected from porous Ti 73.8 Ni 26.2 , and the pore size of the porous Ti-Ni alloy is 2 microns;
[0095] Auxiliaries include the following components by weight:
[0096] 13.5 parts of filler;
[0097] 1 part adhesive;
[0098] 0.5 parts of dispersant; and,
[0099] The filler is selected...
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