A kind of preparation method of 550 ℃ ~ 650 ℃ high temperature titanium alloy foil
A high-temperature titanium alloy and titanium alloy technology, applied in metal rolling, metal processing equipment, weight reduction, etc., to achieve the effect of weakening rolling texture, refining grain size, and weakening transformation texture
Active Publication Date: 2022-05-31
INST OF METAL RESEARCH - CHINESE ACAD OF SCI
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AI Technical Summary
Problems solved by technology
[0004] Existing patents at home and abroad rarely involve the preparation process and method of high-temperature titanium alloy foils at 550°C to 650°C. The demand is becoming more and more urgent. It not only requires high-temperature titanium alloy foil to have good formability, but also requires high tensile strength at room temperature and high temperature (550 ° C ~ 650 ° C)
Method used
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Experimental program
Comparison scheme
Effect test
Embodiment 1
[0048] The TA32 (Ti55) titanium alloy foil with a thickness of 0.1 mm prepared in this example has an average grain size of 3 μm to 5 μm
Embodiment 2
[0062] The TA33 (Ti60) titanium alloy foil with a thickness of 0.2 mm prepared in this example has an average grain size of 4 μm to 6 μm
Embodiment 3
[0075] Step eleven, the foil in the rolled state is put into a vacuum furnace to carry out 900 ° C, 90min vacuum annealing heat treatment,
[0076] The Ti65 titanium alloy foil with a thickness of 0.08 mm prepared in this example has an average grain size of 5 μm to 8 μm, and
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Abstract
A method for preparing a high-temperature titanium alloy foil at 550°C to 650°C, specifically: (1) heating a high-temperature titanium alloy ingot at 1100°C to 1200°C and then forging to obtain a blank; Rolling after heating; (3) water quenching and cooling to room temperature after heat treatment at 50°C to 70°C above the β transformation point to obtain a slab; (4) rolling at 950°C to 1000°C; (5) Assembling and welding the obtained billets to obtain clad rolling ladles; (6) heating the lamination ladles at 950°C to 1000°C, and then rolling; (8) After heating the ladle at 900°C to 950°C, roll it perpendicular to the previous rolling direction; (9) annealing, creep correction, alkali pickling and After sanding, obtain a plate with a thickness of 0.6mm; (10) cut the plate and perform 7 to 25 times of cold rolling to obtain a rolled foil with a thickness of 0.08mm to 0.2mm; (11) perform vacuum annealing heat treatment, A finished foil material with a thickness of 0.08mm-0.2mm is obtained.
Description
A kind of preparation method of 550 ℃~650 ℃ high temperature titanium alloy foil technical field [0001] The present invention belongs to the technical field of titanium alloy material processing, in particular to a 550 ℃~650 ℃ high temperature titanium alloy foil material preparation method. Background technique [0002] 550 ℃ ~ 650 ℃ high temperature titanium alloy is mainly used in the high temperature of aero engines and aerospace hypersonic vehicles. structural components. At present, my country's self-developed high-temperature titanium alloys include TA32, TA33 and Ti65 titanium alloys, which can be used for a long time. 550 ℃, 600 ℃ and 650 ℃ respectively, the above high temperature titanium alloy plates have been used in aero-engines and supersonic aircrafts The thermal structure components such as the cylinder, body, and wings. [0003] The high temperature bearing structure of the high temperature titanium alloy foil with a temperature of 550 ° C to 650 ° C ...
Claims
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Patent Timeline
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IPC IPC(8): B21B1/40B21B1/38B21C37/02B21J5/00C22F1/18C22F1/02
CPCB21B1/40B21B1/38B21C37/02B21J5/002C22F1/183C22F1/02B21B2001/386Y02T50/40
Inventor 王清江陈志勇刘建荣朱绍祥
Owner INST OF METAL RESEARCH - CHINESE ACAD OF SCI