Hydrocracking catalyst and preparation method and application thereof
A hydrocracking and catalyst technology, applied in physical/chemical process catalysts, molecular sieve catalysts, chemical instruments and methods, etc., can solve problems such as low yield of light oil and small pore volume of catalysts
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Embodiment 1
[0033] (1) Weigh 20 g of Y molecular sieves and add them into the reaction kettle according to the amount that the total weight of the molecular sieves accounts for 50 wt% of the weight of the composite material.
[0034] (2) The solid aluminum sulfate is prepared into 500mL concentration of 20g Al 2 o 3 The aluminum sulfate solution (a) of / L is added the dilute ammonia solution (b) of 10wt% by adding an appropriate amount of deionized water to the concentrated ammonia water, gets the concentrated water glass solution and adds an appropriate amount of deionized water to be diluted into the water glass solution of 72mL 14wt% ( c).
[0035] (3) Add 100mL of deionized water to the reaction kettle and heat it to 75°C, add (a) and (b) at the same time, adjust the pH between 8 and 9 for gelation for 30 minutes, and keep the temperature constant after the feeding is completed , aging for 30min.
[0036] (4) After the aging is completed, add (c) into the aged solution, keep the te...
Embodiment 2
[0042] (1) According to the addition amount of molecular sieve weight totaling 50wt% of composite material weight, Y molecular sieve and β molecular sieve weight ratio is 7:3, respectively weigh 14g Y molecular sieve and 6gβ molecular sieve and add into the reaction kettle.
[0043] (2) The solid aluminum sulfate is prepared into 500mL concentration of 20g Al 2 o 3 The aluminum sulfate solution (a) of / L is added the dilute ammonia solution (b) of 10wt% by adding an appropriate amount of deionized water to the concentrated ammonia water, gets the concentrated water glass solution and adds an appropriate amount of deionized water to be diluted into the water glass solution of 72mL 14wt% ( c).
[0044] (3) Add 100mL of deionized water to the reaction kettle and heat it to 75°C, add (a) and (b) at the same time, adjust the pH between 8 and 9 for gelation for 30 minutes, and keep the temperature constant after the feeding is completed , aging for 30min.
[0045] (4) After the a...
Embodiment 3
[0051] (1) According to the addition amount that the total weight of molecular sieve accounts for 50wt% of the weight of the composite material, and the weight ratio of Y molecular sieve and β molecular sieve is 1:1, weigh 10g of Y molecular sieve and 10g of β molecular sieve into the reaction kettle respectively.
[0052] (2) The solid aluminum sulfate is prepared into 500mL concentration of 20g Al 2 o 3 The aluminum sulfate solution (a) of / L is added the dilute ammonia solution (b) of 10wt% by adding an appropriate amount of deionized water to the concentrated ammonia water, gets the concentrated water glass solution and adds an appropriate amount of deionized water to be diluted into the water glass solution of 72mL 14wt% ( c).
[0053] (3) Add 100mL of deionized water to the reaction kettle and heat it to 75°C, add (a) and (b) at the same time, adjust the pH between 8 and 9 for gelation for 30 minutes, and keep the temperature constant after the feeding is completed , a...
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