Electrolyte membrane for all-solid-state battery, and all-solid-state battery comprising same
A solid electrolyte membrane and solid-state battery technology, applied in the direction of solid electrolyte, electrolyte, non-aqueous electrolyte, etc., can solve problems such as explosion, fire, and damage to solid electrolyte membranes, prevent thermal runaway and explosion, and improve heat resistance and safety sexual effect
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Embodiment 1
[0081] First, polystyrene-polyethylene oxide block copolymer (polystyrene-co-polyethylene oxide, PS-b-PEO, room temperature ionic conductivity: 8 × 10 -8 S / cm) and polyethylene oxide (PEO, molecular weight (Mn): 600 kg / mol) were introduced into tetrahydrofuran (THF) as a solvent at a weight ratio of 2:8 to prepare a 5% by weight polymer solution. Here, PS-b-PEO is a copolymer including polystyrene (PS) blocks and polyethylene oxide (PEO) blocks, the blocks being bonded to each other at their respective terminals. In this copolymer, the PS block has a molecular weight (Mn) of 60 kg / mol and the PEO block has a molecular weight (Mn) of 18 kg / mol. Here, LiTFSI as a lithium salt is also represented by [EO] / [Li + ]=18 / 1 molar ratio is introduced. The polymer solution was stirred overnight at 60 °C so that the PS-b-PEO, PEO and lithium salt introduced therein could be fully dissolved. The polymer solution was coated by spin coating at 1000 rpm for 1 min and dried under vacuum over...
Embodiment 2
[0083] A solid electrolyte membrane was obtained in the same manner as in Example 1, except that PS-b-PEO and PEO were used in a weight ratio of 4:6, and the thickness of the obtained solid electrolyte membrane was 30 μm.
Embodiment 3
[0085]A solid electrolyte membrane was obtained in the same manner as in Example 1, except that PS-b-PEO and PEO were used in a weight ratio of 5:5, wherein PS-b-PEO was composed of polystyrene (PS) blocks and Copolymer of polyethylene oxide (PEO) blocks (the blocks are bonded to each other at their respective ends), the PS block has a molecular weight (Mn) of 26 kg / mol and an ionic conductivity of 5×10 - 7 S / cm (room temperature), the molecular weight (Mn) of the PEO block is 32 kg / mol, and the thickness of the obtained solid electrolyte membrane is 30 μm.
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