Online analysis and detection device and method for heated cigarette smoke

A cigarette smoke and detection device technology, which is applied in the field of online analysis and detection devices for heated cigarette smoke, can solve problems such as blank research, avoid the use of toxic organic solvents, improve instrument measurement precision, and reduce pipeline pollution Effect

Pending Publication Date: 2022-01-25
CHINA TOBACCO HUNAN INDAL CORP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, research on online analysis methods for heated cigarette smoke is still blank

Method used

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  • Online analysis and detection device and method for heated cigarette smoke
  • Online analysis and detection device and method for heated cigarette smoke
  • Online analysis and detection device and method for heated cigarette smoke

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0090] On-line detection of whole smoke components of heated cigarettes.

[0091] Gas chromatography mass spectrometer (GC / MS) is used as the analysis detector, and the online analysis device adopts figure 1 The online analysis and detection device shown. The volume of the sample quantitative loop is 0.5mL, the internal standard gas is ethanol standard gas, the volume of the internal standard sample quantitative loop is 0.25mL, and the insulation temperature of the transmission line is 150°C.

[0092] Heated cigarette sample preparation and smoking: Before the experiment, the heated cigarette sample was placed in a constant temperature and humidity condition of temperature (22±1)°C and relative humidity (60±2)% for 48 hours. The suction parameters were a suction volume of 55 mL, a suction duration of 2 s, a suction interval of 30 s, and a bell-shaped suction curve.

[0093] GC conditions: Agilent DB-WAXETR quartz capillary column (60m×250μm×0.25μm); inlet temperature 250°C; ...

Embodiment 2

[0098] Puff-by-puff analysis of heated cigarette smoke

[0099] Example 1 was repeated according to the same steps described above, and the sample quantification loop captured the flue gas port by port according to the suction port sequence for online analysis.

Embodiment 3

[0101] On-line detection of gas phase components in heated cigarette smoke.

[0102] Example 1 was repeated according to the same steps described above, a Cambridge filter was added to the cigarette holder, and the vapor phase of the heated cigarette smoke was analyzed on-line.

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Abstract

The invention discloses an on-line analysis and detection device and method for heated cigarette smoke. The device comprises a cigarette holder, a cigarette smoking module, an on-line sampling module, an on-line internal standard introduction module, an on-line smoke analysis module, a flow path system and a control module. The cigarette holder, the cigarette smoking module, the on-line introduction internal standard module and the on-line smoke analysis module are communicated with the on-line sampling module through the flow path system, and the on-line introduction internal standard module is further used for being communicated with external carrier gas; the on-line sampling module is used for collecting a smoke sample and introducing the smoke sample into the on-line smoke analysis module; the on-line internal standard introduction module is used for collecting an internal standard gas sample and introducing the internal standard gas sample into the on-line flue gas analysis module; and the on-line smoke analysis module is used for receiving the smoke sample and the internal standard gas sample to carry out smoke on-line analysis and detection. Internal standard gas is quantitatively introduced into the on-line flue gas analysis module through the on-line internal standard introduction module, so that the sample introduction amount can be ensured to be accurate, and the detection precision is improved; the smoke sample does not need to be subjected to any sample pretreatment, and simplicity, convenience and high efficiency are achieved.

Description

technical field [0001] The invention relates to the technical field of on-line analysis of heated cigarette smoke, in particular to an on-line analysis and detection device and method for heated cigarette smoke. Background technique [0002] In recent years, heated tobacco product (HTP) uses an external heat source to heat the cut tobacco (200-350°C) instead of directly burning the cigarette, which reduces the harmful components produced by the high-temperature (up to 900°C) combustion and cracking of tobacco. It is most similar to traditional cigarettes and is favored by consumers. [0003] Smoke is the most important characteristic of tobacco products for consumers, and the most important factor reflecting the quality level and style characteristics of tobacco products. The analysis of the chemical components of smoke is a very important basic research work. Heating cigarettes that generate aerosols by heat distillation may contain less tobacco pyrolysis and combustion de...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/02
CPCG01N30/02G01N2030/045
Inventor 邓婷庹苏行杨华武杜文谭新良刘建福
Owner CHINA TOBACCO HUNAN INDAL CORP
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