Hollow particles, preparation method therefor, and heat-radiating fluid composition comprising same
A technology of hollow particles and heat-conducting fluid, applied in chemical instruments and methods, microsphere preparation, ceramic products, etc., can solve the problems of reduced heat dissipation characteristics, low heat dissipation performance, insufficient heat dissipation capacity, etc., achieve excellent heat dissipation performance and improve heat dissipation performance Effect
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Embodiment 1
[0104] (1) Preparation of Hollow Particle I
[0105] In the average particle size of 100g (D 50 ) of 1 μm in styrene spherical particles were treated with 500 g of sulfuric acid and thus modified the surface of the particles with anions, 25 g of carbon nanotubes (LG Chem) were added.
[0106] The carbon-treated styrene spherical particles were immersed in 100 ml of ATSB solution, thereby introducing alumina precursor cations (Al 3+ ).
[0107] Styrene spherical particles treated with carbon and into which alumina precursor cations were introduced were heat-treated at 800° C. for 1 hour under an oxygen condition, thereby forming on the surface of the particles a compound containing alumina and carbon in a weight ratio of 4:1 The inorganic particle layer of nanotubes, meanwhile, obtains hollow inorganic particles in which empty inner spaces are formed inside the inorganic particle layer.
[0108] Hollow inorganic particles were immersed in a binding resin solution (20% (w / w) ...
Embodiment 2
[0112] A hollow particle II and a heat dissipation fluid composition were prepared in the same manner as in Example 1, except that tetrachlorosilane solution was used instead of the ATSB solution used in Example 1, and graphene was used instead of carbon nanotubes.
Embodiment 3
[0114] In addition to the preparation of hollow particles when the inorganic particle layer comprising aluminum oxide and carbon nanotubes with a weight ratio of 4:1 is formed on the surface of the particle in Example 1, the hollow particle is formed on the surface of the particle and contains a weight ratio of 3 In addition to preparing hollow inorganic particles during the inorganic particle layer of aluminum oxide and carbon nanotubes of 1, hollow particles III and heat dissipation fluid composition were prepared in the same manner as in Example 1.
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