MOF [CuBTA2] (Hgua) 2 * xH2O compound and application thereof
A compound and reaction technology, which is applied in the field of green combustion catalysts, can solve problems such as adverse effects on the energy performance of propellants, and achieve the effects of increased burning rate, simple preparation process, and high yield
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Embodiment 1
[0021] The example MOF[CuBTA 2 ] (Hgua) 2 2H 2 Preparation of O:
[0022] Disperse 1,1'-bis(1-H-tetrazole)amine (16.92g, 0.11mol) in deionized water (500mL) at room temperature, and add potassium hydroxide (12.06g, 0.22mol) to form a pH value of 10.2 transparent solution; after heating up to 70°C, add guanidine hydrochloride (26.52g, 0.28mol) and copper chloride dihydrate (9.38g, 0.055mol) to the above solution, then cool down naturally to precipitate a black precipitate; then use the precipitate The energetic MOF [CuBTA 2 ] (Hgua) 2 2H 2 O (20.8 g), 72.0% yield.
Embodiment 2
[0024] The difference between this example and Example 1 is that the pH value is 9.0, and the product yield is 50.8%.
Embodiment 3
[0026] The difference between this example and Example 1 is that the reaction is carried out after the temperature is raised to 90° C., and the yield of the obtained product is 65%.
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