Temperature self-adaptive intelligent window and preparation method thereof
A self-adaptive, smart window technology, applied in instruments, optics, nonlinear optics, etc., can solve the problems of high low critical phase transition temperature value, poor sunlight modulation efficiency, slow phase transition rate, etc., and achieves simple preparation method, Good indoor lighting, fast speed effect
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Embodiment 1
[0045] As an embodiment of a temperature-adaptive smart window of the present invention, the specific implementation process of the temperature-adaptive smart window is as follows:
[0046] (1) Weigh 5.700g N-isopropylacrylamide, 0.033g N,N'-methylenebisacrylamide and 0.020g sodium dodecyl sulfate, dissolve them in 120mL ultrapure water, put the reaction solution in Put it in a 70°C water bath and continue stirring for 1 hour, then dissolve 0.042 g of ammonium persulfate in 10 mL of ultrapure water and add it to the above reaction solution to start the polymerization reaction for 4 hours. After the reaction, it was cooled to room temperature and allowed to stand for a period of time. Then, at room temperature, dialysis and purification, and then air-dried and concentrated to obtain a temperature-sensitive hydrogel with submicron particle size, the mass fraction of the temperature-sensitive hydrogel is 5% of the total solution after dialysis purification and concentration.
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Embodiment 2
[0050] As an embodiment of a temperature-adaptive smart window of the present invention, the specific implementation process of the temperature-adaptive smart window is as follows:
[0051] (1) Weigh 5.700g N-isopropylacrylamide, 0.033g N,N'-methylenebisacrylamide and 0.020g sodium dodecyl sulfate, dissolve them in 120mL ultrapure water, put the reaction solution in Put it in a 70°C water bath and continue stirring for 1 hour, then dissolve 0.042 g of ammonium persulfate in 10 mL of ultrapure water and add it to the above reaction solution to start the polymerization reaction for 4 hours. After the reaction, it was cooled to room temperature and allowed to stand for a period of time. Then, at room temperature, dialysis and purification, and then air-dried and concentrated to obtain a temperature-sensitive hydrogel with submicron particle size, the mass fraction of the temperature-sensitive hydrogel is 5% of the total solution after dialysis purification and concentration.
[...
Embodiment 3
[0055] As an embodiment of a temperature-adaptive smart window of the present invention, the specific implementation process of the temperature-adaptive smart window is as follows:
[0056] (1) Weigh 5.700g N-isopropylacrylamide, 0.033g N,N'-methylenebisacrylamide and 0.025g sodium dodecyl sulfate, dissolve them in 120mL ultrapure water, put the reaction solution in Put it in a 70°C water bath and continue stirring for 1 hour, then dissolve 0.042 g of ammonium persulfate in 10 mL of ultrapure water and add it to the above reaction solution to start the polymerization reaction for 4 hours. After the reaction, it was cooled to room temperature and allowed to stand for a period of time. Then, at room temperature, dialysis and purification, and then air-dried and concentrated to obtain a temperature-sensitive hydrogel with submicron particle size, the mass fraction of the temperature-sensitive hydrogel is 5% of the total solution after dialysis purification and concentration.
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