High-solid-content crystal combination porcelain feed and preparation method thereof

A technology of high solid content and crystal porcelain, which is applied in the appearance structural parts of crystal porcelain, high solid content composite crystal porcelain feeding and its preparation, can solve the problems of single color of the shell, small cutting amount, low strength, etc., and reduce the manufacturing cost. Low cost, good size processing, and low surface hardness

Pending Publication Date: 2022-07-05
南通通州湾新材料科技有限公司 +1
View PDF5 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to its shielding effect, traditional metal poses a huge challenge to antenna design. It will not be used in the manufacture of 5G backplanes (housings), while plastics are inherently low-strength and non-wear-resistant, which limits their use in large-size screens, ultra- In addition, with the improvement of consumer aesthetics, the traditional single metal shell and plastic backplane (shell) will also be difficult to impress consumers.
[0003] In the patent application number 201510940002.3, it is reported that the method of injection molding and sintering the zirconia powder and the binder to obtain the feed is used to prepare the mobile phone shell in the field of consumer electronics. This scheme uses ZrO 2 Ceramics have the characteristics of good hardness and high wear resistance, but the preparation of mobile phone casings also has the following disadvantages: 1) the fracture toughness of ceramics is still far lower than that of metal and plastic parts, and large-scale impact resistance such as the prepared mobile phone backplane (shell) Poor drop performance, easy to break; 2) ZrO 2 The density of ceramics is as high as 6.1g / cm 3 , the quality of the large-sized parts of the back plate of the mobile phone (housing) is heavy, which is not conducive to the development of thinner and lighter consumer electronics; 3) the color of the ceramic case is single, and if a small amount of colorant is added during the firing process, the quality of the parts will also be deteriorated. Mechanical properties, resulting in monotonous color of the ceramic (housing) backplane
[0004] On the other hand, the Mohs hardness of pure zirconia ceramics is close to 9, which is second only to diamond, resulting in low cutting volume, small amount of cutting, difficult processing and long processing time in the grinding and polishing process. Only the machining cost of zirconia ceramic back cover It accounts for 2 / 3 of the entire production cost, and the processing process is easy to break, and the yield rate is low

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • High-solid-content crystal combination porcelain feed and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0026] The invention discloses a preparation method of high solid content composite crystal ceramic feed, comprising the following steps:

[0027] a) Weigh parts by weight of 25-32.5 parts by weight of the inorganic powder of the first particle size, 25-32.5 parts by weight of the inorganic powder of the second particle size and 35-50 parts by weight of the organic polymer resin to obtain a mixed raw material ;

[0028] b) Banbury or extrude the mixed raw materials obtained in step a).

[0029] In this embodiment, the D50 of the inorganic powder with the first particle size selected in the above-mentioned preparation method of the high-solid content composite ceramic material is 0.7-1.8 μm, and the D50 of the inorganic powder with the second particle size is 0.1-1. 0.3 μm.

[0030] In the present embodiment, in the above-mentioned preparation method of high-solid content composite ceramic feedstock, the weight part of the inorganic powder with the first particle size is 28-3...

Embodiment 1

[0034] Feed preparation with a particle size ratio of 4.5

[0035] Weigh 2kg of zirconia inorganic powder with D50 of about 1.8μm, and then weigh 2kg of zirconia inorganic powder with D50 of about 0.4μm, and mix the two powders uniformly with a small solid mixer for later use.

[0036] Weigh 2.15kg of polyphenylene sulfide and add it to the mixer and heat it up to 310°C to melt it. Add the mixed powder to the mixer for several times, then close the mixer and evacuate to -0.06MPa at 310°C. After mixing for 1 hour, the temperature is lowered and the material is crushed to obtain the feed.

[0037] Melt index meter test Heat to 310 ℃, after heating 150g of the above-mentioned feed melt index meter, test under 2.16kg weight, the melt index is 0.91g / 10min.

Embodiment 2

[0039] Feed preparation with a particle size ratio of 20

[0040]Weigh 2kg of zirconia inorganic powder with D50 of about 1.8μm, and then weigh 2kg of zirconia inorganic powder with D50 of about 0.09μm, and mix the two powders uniformly with a small solid mixer for later use.

[0041] Weigh 2.15kg of polyphenylene sulfide and add it to the mixer and heat it up to 310°C to melt it. Add the mixed powder to the mixer for several times, then close the mixer and evacuate to -0.06MPa at 310°C. After mixing for 1 hour, the temperature is lowered and the material is crushed to obtain the feed.

[0042] Melt index meter test Heating to 310 ℃, after heating 150g of the above-mentioned feed melt index meter, test under 2.16kg weight, the melt index is 0.55g / 10min.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
densityaaaaaaaaaa
melt flow indexaaaaaaaaaa
melt flow indexaaaaaaaaaa
Login to view more

Abstract

The invention provides a high-solid-content crystal combination porcelain feed and a preparation method thereof, and the feed comprises the following components in parts by weight: 25-32.5 parts of inorganic powder with a first particle size, 25-32.5 parts of inorganic powder with a second particle size and 35-50 parts of organic polymer resin, wherein the ratio of the size of the inorganic powder with the first particle size to the size of the inorganic powder with the second particle size is greater than 5.6. Compared with an inorganic powder feed with a single particle size, the feed realizes that the filling weight ratio of the inorganic powder in the feed is greater than 50% and the inorganic powder has good fluidity by limiting the matching of the inorganic powder with different sizes. By utilizing the difference of the flowability of the inorganic powder with different sizes in the feeding process, the gradient distribution of the inorganic powder with large particle size and the inorganic powder with small particle size is realized in the injection molding process, and the technical effect of'tough inside and hard outside 'of the appearance structural member of the crystal combination porcelain can be realized; the method can be used for preparing mobile phone shells, middle frames, integrated mobile phone shell middle frames, watch rear covers and middle frames.

Description

technical field [0001] The invention relates to the technical field of structural parts and their preparation, in particular to the field of preparation of consumer electronic shell structural parts, in particular to a high-solid-content composite crystal ceramic feed and a preparation method thereof, and a composite crystal ceramic appearance structural part. Background technique [0002] With the rapid development of consumer electronics such as mobile phones, the structural components such as the backplane (casing) of consumer electronics have made great progress, but also encountered new problems. In particular, in the future 5G era, more stringent requirements are placed on the material of the consumer electronics backplane (casing). Due to its shielding effect, traditional metal poses a huge challenge to antenna design, and it will not be used in the manufacture of 5G backplanes (housings). Applications in thin fields, and with the improvement of consumer aesthetics, ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): C08L81/02C08L69/00C08K3/22C08K3/36B29B7/00B29C48/00
CPCC08K3/22C08L81/02C08L69/00B29B7/002B29C48/00C08K2201/005C08K2003/2244C08K2003/2227C08K3/36
Inventor 周涛雒文博贺小亮
Owner 南通通州湾新材料科技有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products