Heating body material for low-temperature cigarette as well as preparation method and application of heating body material
A low-temperature cigarette and heating element technology, applied in the field of tobacco products, can solve the problems of lower heating efficiency, high cost, and inability to heat tobacco sheets
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Embodiment 1
[0027] 1) cleaning; the alumina ceramic powder and the ammonium bicarbonate foaming agent are subjected to pickling and ultrasonic cleaning to remove the surface oxide film and pollutants, wherein the volume fraction of the foaming agent is 10%;
[0028] 2) Mixing: Put the above powder into a ball mill tank for mixing. The ratio of ball to material used is 5:1, the rotation speed is 200rpm, the ball milling medium is high-purity ethanol, and the ball milling time is 2h;
[0029] 3) Drying: dry the ball-milled mixed powder in a vacuum drying oven at a temperature of 60°C;
[0030] 4) Molding: the dried powder is sieved and then molded, the compression pressure is 200MPa, and the pressure holding time is 30s;
[0031] 5) Immersion: Put the above-mentioned green compact and Al sheet into a ceramic crucible in a mass ratio of 1:4, and carry out infiltration treatment in a vacuum sintering furnace. The infiltration temperature is 1200°C, the infiltration time is 1h, and the vacuum...
Embodiment 2
[0034] 1) Cleaning; pickling and ultrasonic cleaning zirconia ceramic powder and calcium carbonate foaming agent to remove surface oxide film and pollutants, wherein the volume fraction of foaming agent is 25%;
[0035] 2) Mixing: Put the above powder into a ball mill tank for mixing. The ratio of ball to material used is 7:1, the rotation speed is 500rpm, the ball milling medium is high-purity ethanol, and the ball milling time is 12h;
[0036] 3) Drying: dry the ball-milled mixed powder in a vacuum drying oven at a temperature of 120°C;
[0037] 4) Molding: the dried powder is sieved and then molded, the pressing pressure is 400MPa, and the pressure holding time is 120s;
[0038] 5) Immersion: Put the above-mentioned green compact and nickel sheet into a ceramic crucible in a mass ratio of 1:1, and carry out infiltration treatment in a vacuum sintering furnace. The infiltration temperature is 2000°C, the infiltration time is 10h, and the vacuum degree is 2Pa.
[0039] 6) G...
Embodiment 3
[0041] 1) Cleaning; pickling and ultrasonic cleaning zirconia ceramic powder and calcium carbonate foaming agent to remove surface oxide film and pollutants, wherein the volume fraction of foaming agent is 15%;
[0042] 2) Mixing: Put the above powder into a ball mill tank for mixing. The ratio of ball to material used is 7:1, the rotational speed is 350rpm, the ball milling medium is high-purity ethanol, and the ball milling time is 5h;
[0043] 3) Drying: dry the ball-milled mixed powder in a vacuum drying oven at a temperature of 80°C;
[0044] 4) Molding: the dried powder is sieved and then molded, the compression pressure is 300MPa, and the pressure holding time is 60s;
[0045] 5) Immersion: put the above-mentioned green compact and Ni50Cr50 (mass fraction) alloy wire into a ceramic crucible in a mass ratio of 7:3, and carry out infiltration treatment in a vacuum sintering furnace. The degree of vacuum is 3Pa.
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