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Treatment method and treatment device for water-based waste solvent

A treatment method and waste solvent technology, which is applied in the field of water-based waste solvent treatment method and its treatment device, can solve the problems of affecting membrane separation performance and service life, frequent membrane replacement, and increasing operating costs, so as to achieve environmental reduction and resource efficiency, reduce membrane fouling, and ensure stable operation

Pending Publication Date: 2022-07-22
SHANGHAI ELECTRICGROUP CORP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the existing biochemical methods, low-temperature evaporation technology, advanced oxidation technology, reverse osmosis membrane method and other treatment methods have problems such as too high organic load, azeotropic water and organic matter, unstable operation and high cost, and membrane material life. Engineering application cannot be realized due to various problems
The pervaporation membrane technology that has appeared in recent years can realize the engineering application of the reduction and resource utilization of the aqueous waste solvent, but in the process of practical application, the membrane separation performance decays too fast, resulting in frequent membrane replacement, which greatly Increased operating costs
This is because the curing agent and resin in the water-based waste solvent cannot be completely removed by coagulation and precipitation, and will be precipitated and deposited on the membrane surface after heating, which has a relatively large negative impact on the separation performance and service life of the pervaporation membrane.
[0004] Aiming at the above-mentioned existing pervaporation technology for treating the water-based waste solvent of automobile painting, the residual curing agent and resin after the coagulation of wastewater affect the separation performance and service life of the membrane, etc., the present invention provides a water-based waste solvent for automobile painting The treatment method and its treatment device greatly reduce the problem of membrane fouling, prolong the life of the membrane, reduce the cost of membrane replacement, and ensure the stable operation of the pervaporation membrane unit

Method used

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  • Treatment method and treatment device for water-based waste solvent
  • Treatment method and treatment device for water-based waste solvent

Examples

Experimental program
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Effect test

Embodiment 1

[0036] like figure 1 As shown, the present embodiment provides a method for treating aqueous waste solvent, the steps comprising:

[0037] S1. The aqueous waste solvent is transported to the coagulation reaction device 1, and an appropriate amount of coagulant is transported to the coagulation reaction device 1. After the aqueous waste solvent is stirred and reacted completely, the supernatant is It is transported to the vacuum distillation device 2, and the sedimented sludge is transported to the filter press device 4;

[0038] Wherein, in the coagulation reaction device 1, the stirring speed is 200r / min~400r / min, the pH of the reaction is 6~8, the reaction time is 15min~45min, and the standing time is 15min~45min;

[0039] S2, after the precipitation sludge is completed by pressure filtration, the filtrate is transported to the vacuum distillation device 2, and the mud cake is transported to the external treatment section;

[0040] Wherein, in the vacuum distillation devic...

Embodiment 2

[0045] like figure 2 As shown, this embodiment provides an aqueous waste solvent treatment system, which is suitable for the treatment method described in Embodiment 1, including: a coagulation reaction device 1, a vacuum distillation device 2, a pervaporation device 3, and a filter press device 4. Stirring device 5, heating device 6, first liquid storage device 7, second liquid storage device 8, third liquid storage device 9, fourth liquid storage device 10, first liquid pump 11, second liquid pump 12, The third liquid pump 13, the fourth liquid pump 14, the fifth liquid pump 15 and the sixth liquid pump 16;

[0046] Wherein, the first liquid storage device 7 is connected to the coagulation reaction device 1 , the liquid outlet of the coagulation reaction device 1 is connected to the vacuum distillation device 2 , and the second liquid outlet of the vacuum distillation device 2 is connected to the vacuum distillation device 2 . A liquid outlet is connected to the second liq...

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Abstract

The invention relates to a water-based waste solvent treatment method and a treatment device thereof.The treatment method comprises the steps that a water-based waste solvent is conveyed into a coagulation reaction device, a proper amount of coagulant is conveyed into the coagulation reaction device, and after the water-based waste solvent is stirred and completely reacts, the coagulant is added into the coagulation reaction device; conveying the supernatant into a reduced pressure distillation device; after the reduced pressure distillation of the supernatant liquid and the filtrate is completed, conveying a distilled thin liquid into a pervaporation device; after pervaporation of the distilled thin liquid is completed, the pervaporation thin liquid is conveyed to a wastewater treatment workshop section. The invention provides a water-based waste solvent treatment method and a water-based waste solvent treatment device, which can greatly reduce the problem of membrane pollution, prolong the service life of a membrane, reduce the cost of membrane replacement and ensure the stable operation of a pervaporation membrane unit.

Description

technical field [0001] The invention relates to the technical field of industrial wastewater treatment, in particular to a treatment method and a treatment device for an aqueous waste solvent. Background technique [0002] In recent years, with the rapid development of automobile demand, the production lines of many automobile manufacturers are constantly expanding, which has also resulted in a large amount of waste water in automobile painting workshops, including the use of water-based solvents to clean spray guns and pipelines for conveying paint. Aqueous waste solvent produced during The water-based waste solvent mainly contains complex components such as paint, organic solvent, surfactant and curing agent, and the CODcr content is about 300,000 to 800,000 mg / L. At present, according to feedback from major painting workshops, this water-based waste solvent is basically entrusted to qualified companies for incineration treatment as hazardous waste, and the treatment cost...

Claims

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Application Information

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IPC IPC(8): C02F9/10C02F11/122C02F1/04C02F1/44C02F1/52C02F101/30C02F101/34C02F103/14
CPCC02F9/00C02F11/122C02F1/448C02F1/04C02F1/5281C02F2101/30C02F2101/301C02F2101/34C02F2103/14C02F2209/08
Inventor 尹竞黄思远何龙黄磊张静姚迎迎
Owner SHANGHAI ELECTRICGROUP CORP
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