Oil-resistant deformable plugging particle and preparation method thereof
A particle and oil-resistant technology, applied in chemical instruments and methods, drilling compositions, etc., can solve the problems of oil-based drilling fluid wellbore leakage, economic loss, shortage, etc., and achieve good elastic deformation ability and plugging performance, Good oil resistance and high pressure bearing capacity
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Embodiment 1
[0023] An oil-resistant deformable plugging particle, the inner core is an elastic-plastic rubber particle, and the outer shell is coated with a fluoropolymer. Wherein, the rubber particles are natural rubber, and the particle size ranges from 1 to 3 mm.
[0024] The preparation method of the oil-resistant deformable plugging particles includes:
[0025] (1) Select uniform rubber particles with a particle size range of 1-3mm to clean and dry;
[0026] (2) Spray the rubber particles with 8% acetic acid solution and 5% glycerol solution successively, and keep turning the rubber particles during the spraying process to ensure that the surfaces of all rubber particles are fully wetted;
[0027] (3) Put the wetted rubber particles on the temperature-controlled ultrasonic vibrating screen, and the mesh of the screen cloth is smaller than the diameter of the rubber particles to prevent leakage;
[0028] (4) Open the ultrasonic vibrating screen, control the ultrasonic frequency betw...
Embodiment 2
[0031] An oil-resistant deformable plugging particle, the inner core is an elastic-plastic rubber particle, and the outer shell is coated with a fluoropolymer. Among them, the rubber particles are natural rubber, and the particle size range is 3-5mm.
[0032] The preparation method of the oil-resistant deformable plugging particles includes:
[0033] (1) Select uniform rubber particles with a particle size range of 3-5mm to clean and dry;
[0034] (2) Spray the rubber particles with 8% acetic acid solution and 5% glycerol solution successively, and keep turning the rubber particles during the spraying process to ensure that the surfaces of all rubber particles are fully wetted;
[0035] (3) Put the wetted rubber particles on the temperature-controlled ultrasonic vibrating screen, and the mesh of the screen cloth is smaller than the diameter of the rubber particles to prevent leakage;
[0036] (4) Open the ultrasonic vibrating screen, control the ultrasonic frequency between ...
Embodiment 3
[0039] An oil-resistant deformable plugging particle, the inner core is an elastic-plastic rubber particle, and the outer shell is coated with a fluoropolymer. Wherein, the rubber particles are natural rubber, and the particle size ranges from 1 to 3 mm.
[0040] The preparation method of the oil-resistant deformable plugging particles includes:
[0041] (1) Select uniform rubber particles with a particle size range of 1-3mm to clean and dry;
[0042] (2) Spray the rubber particles with 8% acetic acid solution and 5% glycerol solution successively, and keep turning the rubber particles during the spraying process to ensure that the surfaces of all rubber particles are fully wetted;
[0043] (3) Put the wetted rubber particles on the temperature-controlled ultrasonic vibrating screen, and the mesh of the screen cloth is smaller than the diameter of the rubber particles to prevent leakage;
[0044] (4) Open the ultrasonic vibrating screen, control the ultrasonic frequency betw...
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