Production process of photosensitive monomer material
A technology of photosensitive monomer and production process, applied in the direction of photosensitive materials for opto-mechanical equipment, etc., can solve the problems of inconvenience for large-scale mass production of enterprises and high price of polymer materials, achieve low production cost and improve molding processing performance. , the effect of good photosensitive performance
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Embodiment 1
[0022] Example 1, please refer to figure 1 , the present invention provides a technical scheme: the production process of the photosensitive monomer material, comprising the following steps:
[0023] S1: Solution adjustment, first take deionized water and photosensitive resin, dilute to 155ml / l working solution when using, then measure pH with acidity meter, then adjust pH, then take acrylamide and diacetone acrylamide, after obtaining the acrylamide and diacetone acrylamide in conditioned deionized water:
[0024] S2: Mixing reaction, then weigh the initiator and add it into the reaction kettle, and gradually increase the temperature of the reaction kettle itself, and keep it for 4 hours. After the maintenance, the initiator is added to the reaction kettle again, and the polymerization operation is carried out for 10 hours to obtain the photosensitive polymer:
[0025] S3: Fine treatment, then add defoaming agent to the reaction kettle, and continuously defoaming the solutio...
Embodiment 2
[0035] Example 2, please refer to figure 1 , the present invention provides a technical scheme: the production process of the photosensitive monomer material, comprising the following steps:
[0036] S1: Solution adjustment, first take deionized water and photosensitive resin, dilute to 120ml / l working solution when using, then measure pH with acidity meter, then adjust pH, then take acrylamide and diacetone acrylamide, after obtaining acrylamide and diacetone acrylamide in conditioned deionized water:
[0037] S2: Mixing reaction, then weigh the initiator and add it to the reaction kettle, and gradually increase the temperature of the reaction kettle itself, and keep it for 3 hours. After the maintenance, the initiator is added to the reaction kettle again, and the polymerization operation is carried out for 8 hours to obtain the photosensitive polymer:
[0038] S3: Fine treatment, then add defoaming agent to the reaction kettle, and continuously defoaming the solution in th...
Embodiment 3
[0048] Example three, please refer to figure 1 , the present invention provides a technical scheme: the production process of the photosensitive monomer material, comprising the following steps:
[0049] S1: Solution adjustment, first take deionized water and photosensitive resin, dilute to 200ml / l working solution when using, then measure pH with acidity meter, then adjust pH, then take acrylamide and diacetone acrylamide, after obtaining the acrylamide and diacetone acrylamide in conditioned deionized water:
[0050] S2: Mixing reaction, then weigh the initiator and add it to the reaction kettle, and gradually increase the temperature of the reaction kettle itself, and keep it for 4 hours. After holding, the initiator is added to the reaction kettle again, and the polymerization operation is carried out for 8 hours to obtain the photosensitive polymer:
[0051] S3: Fine treatment, then add defoaming agent to the reaction kettle, and continuously defoaming the solution in th...
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