Analysis method of packed column gas chromatography for hydrogen peroxide operating fluid

A gas chromatographic analysis, gas chromatographic technology, applied in the field of analysis of hydrogen peroxide working fluid, to achieve the effect of good reproducibility, high sensitivity and simple method
CN1424580AInactive Publication Date: 2003-06-18中国石油化工股份有限公司巴陵分公司

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
中国石油化工股份有限公司巴陵分公司
Publication Date
2003-06-18
Estimated Expiration
Not applicable · inactive patent
Patent Text Reader

Abstract

The present invention relates to the analysis method of filling cylinder gas chromatography for oxydol working liquid. The method is characterized in that toluene is used as a solution, OV-17 as the fixing liquid for the cylinder of gas chromatography. The gas chromatography quantitative analysis for 2-ethyl-anthraquinone and tetrahydro-2-ethyl antraquinone is performed using filling cylinder made of stainless steel and FID sensor. The method is of high sensitivity and high accuracy and has simple and convenient operation.
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Description

technical field

[0001] The invention relates to an analysis method for hydrogen peroxide working liquid by packed column gas chromatography. Background technique

[0002] As a green chemical, hydrogen peroxide will continue to develop vigorously as a key project during the "Tenth Five-Year Plan" period. The production method of hydrogen peroxide is mainly the anthraquinone method, and the essence of the hydrogen peroxide production process by the anthraquinone method is: tetrahydro 2-ethylanthraquinone and 2-ethylanthraquinone (hereinafter referred to as anthraquinone) as working substances , dissolved in an organic solvent to form a working solution, anthraquinone is alternately hydrogenated and oxidized, and hydrogen peroxide is generated at the same time. Whether it is the production process or the laboratory catalytic process research, it is necessary to accurately determine the concentration of tetrahydro 2-ethylanthraquinone and 2-ethylanthraquinone in the working sol...

Claims

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