Method for producing low water peak optic fiber prefabricated piece
A technology of optical fiber prefabricated parts and manufacturing methods, applied in the field of optical fibers, can solve the problems of reducing water peak attenuation, reducing the OH content of optical fiber preforms, and the halogenation dehydration method cannot meet the requirements, so as to achieve the effect of reducing water content and reducing light attenuation
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Embodiment 4
[0047] Example 4, a cylindrical porous prefabricated core rod loose body made in a conventional manner is placed above the interior of the sintering furnace, and the temperature is kept at about 1200-1300 ° C. At the beginning, it is pre-purged with He with a flow rate of 30 SLPM Porous preform mandrel loose body about 15 minutes. After purging, pass through the desiccant Cl 2 Drying was carried out for 60 minutes. During the flow rate of 0.25SLPM Cl 2 And the He of 20SLPM flows through the sintering furnace; After that, the He purging sintering furnace with the flow rate of 30SLPM for 15 minutes; Then, the deuterium gas (D of 0.4SLPM 2 ) and 3~4SLPM flow through D 2 Carrier gas He (containing D 2 O gas) is passed into the sintering furnace at the same time, together with the He flow of 20 SLPM, the mixed gas is used to purge the preform for more than 60 to 360 minutes; the loose body of the porous preform mandrel is lowered to enter the hot zone of the furnace, and the He...
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