Preparation method of nano-gold particle
A gold nanoparticle and gold particle technology, applied in the field of gold nanoparticle preparation, can solve problems such as many steps, and achieve the effects of fast reaction, low preparation cost and mild reaction conditions
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[0011] see figure 1 , so that the HAuCl 4 Add basic CH 3 NO 2 aqueous solution as an example, 0.6 μl CH 3 NO 2 Dissolve in 5ml of distilled water to make nitromethane aqueous solution, stir and add 20μl of 1mol / l NaOH or KOH aqueous solution, the pH value of the solution is 11.06, after stirring for 2 minutes, add 25μL of 24mmol / l HAuCl 4 The aqueous solution has obvious color change within a few seconds, and the light brown gold nanoparticle hydrosol obtained by continuing to stir for 30 minutes.
[0012] Using the above method, changing the pH value of the solution can obtain hydrosols of different colors. For example, when the volumes of 1mol / l NaOH aqueous solution are added to 20 μl, 40 μl, 60 μl and 80 μl respectively, the pH values of the solutions are 11.06, 11.82, 12.26 and 12.43 respectively, and the colors of the aqueous sols of gold nanoparticles thus prepared are orange in turn. , Red, Purple And Blue.
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