The application discloses a preparation method of gold
powder for thick film
conductive paste, and the method comprises the following steps: firstly, dissolving gold blocks in
aqua regia, adding
ammonium chloride, and evaporating to prepare
ammonium chloraurate
powder; secondly, mixing the
ammonium chloraurate
powder with
ascorbic acid and ball milling to obtain uniformly mixed gold-containing precursor powder; thirdly, calcining the gold-containing precursor powder at low temperature in air to obtain nanometer gold powder; and fourthly, adding the nanometer gold powder into
anhydrous ethanol to prepare nanometer gold suspension, and then performing high-temperature atomization to obtain spherical gold powder. By controlling the ball milling time of the ammonium chloraurate and
ascorbic acid, combining with the control of low-temperature
calcination parameters and the temperature of high-temperature atomization, the gold powder for thick film
conductive paste is finally obtained, the addition and cleaning of a direct liquid-phase reduction gold powder dispersant are avoided, the
spherical morphology and high purity of the gold powder are ensured, the gold powder is suitable for thick film conductive use, the preparation method is simple in process, high in product yield, large in output, green in environment protection, and easy for industrial production.