Manufacturing method for protein short staples
A manufacturing method and short fiber technology are applied in the field of material manufacturing and can solve the problems affecting the use range of silkworm chrysalis protein and the like
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Embodiment 1
[0014] A method for manufacturing short protein fibers, which is characterized in that it includes the following production steps: dissolving, alkylation reaction to prepare pupa protein spinning solution, coagulation molding, acetalization treatment, water flow, desulfurization, water washing, pickling and water washing, and Oil, tumble dry.
[0015] The dissolving procedure of the present invention is to take a certain amount of silkworm chrysalis protein and dissolve it in 0.8% sodium hydroxide solution, and the ratio of silkworm chrysalis protein to sodium hydroxide is 1.0:0.15. .
[0016] The process of preparing pupae protein spinning liquid by the alkylation reaction of the present invention is to add silkworm pupae protein into 1.0‰ hydrogen peroxide at a certain temperature for initiation, and then add acrylamide according to the ratio of silkworm pupae protein: acrylamide of 1.0:0.15. After the carbamoyl ethylation reaction, the pupa protein spinning solution was ob...
Embodiment 2
[0023] A method for manufacturing short protein fibers, which is characterized in that it includes the following production steps: dissolving, alkylation reaction to prepare pupa protein spinning solution, coagulation molding, acetalization treatment, water flow, desulfurization, water washing, pickling and water washing, and Oil, tumble dry.
[0024] The dissolving procedure of the present invention is to take a certain amount of silkworm chrysalis protein and dissolve it in 1.5% sodium hydroxide solution, and the ratio of silkworm chrysalis protein to sodium hydroxide is 1.0:0.05. .
[0025] The process of producing pupa protein spinning solution by the alkylation reaction of the present invention is to add silkworm pupa protein to 0.5‰ hydrogen peroxide at a certain temperature for initiation, and then add acrylamide according to the ratio of silkworm pupa protein: acrylamide of 1.0:0.05. After the carbamoyl ethylation reaction, the pupa protein spinning solution was obtai...
Embodiment 3
[0031] A method for manufacturing short protein fibers, which is characterized in that it includes the following production steps: dissolving, alkylation reaction to prepare pupa protein spinning solution, coagulation molding, acetalization treatment, water flow, desulfurization, water washing, pickling and water washing, and Oil, tumble dry.
[0032] The dissolving process of the present invention is to take a certain amount of silkworm chrysalis protein and dissolve it in 1% sodium hydroxide solution, and the ratio of silkworm chrysalis protein to sodium hydroxide is 1.0:0.10. .
[0033] The process of preparing pupae protein spinning solution by the alkylation reaction of the present invention is to add silkworm pupae protein to 0.8‰ hydrogen peroxide at a certain temperature for initiation, and then add acrylamide according to the ratio of silkworm pupae protein: acrylamide of 1.0:0.10. After the carbamoyl ethylation reaction, the pupa protein spinning solution was obtain...
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