Manufacturing method for protein short staples

A manufacturing method and short fiber technology are applied in the field of material manufacturing and can solve the problems affecting the use range of silkworm chrysalis protein and the like

A manufacturing method and short fiber technology are applied in the field of material manufacturing and can solve the problems affecting the use range of silkworm chrysalis protein and the like

CN1584146AActive Publication Date: 2005-02-23YIBIN GRACE
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Experimental program
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Effect test

Embodiment 1

[0014] A method for manufacturing short protein fibers, which is characterized in that it includes the following production steps: dissolving, alkylation reaction to prepare pupa protein spinning solution, coagulation molding, acetalization treatment, water flow, desulfurization, water washing, pickling and water washing, and Oil, tumble dry.

[0015] The dissolving procedure of the present invention is to take a certain amount of silkworm chrysalis protein and dissolve it in 0.8% sodium hydroxide solution, and the ratio of silkworm chrysalis protein to sodium hydroxide is 1.0:0.15. .

[0016] The process of preparing pupae protein spinning liquid by the alkylation reaction of the present invention is to add silkworm pupae protein into 1.0‰ hydrogen peroxide at a certain temperature for initiation, and then add acrylamide according to the ratio of silkworm pupae protein: acrylamide of 1.0:0.15. After the carbamoyl ethylation reaction, the pupa protein spinning solution was ob...

Embodiment 2

[0023] A method for manufacturing short protein fibers, which is characterized in that it includes the following production steps: dissolving, alkylation reaction to prepare pupa protein spinning solution, coagulation molding, acetalization treatment, water flow, desulfurization, water washing, pickling and water washing, and Oil, tumble dry.

[0024] The dissolving procedure of the present invention is to take a certain amount of silkworm chrysalis protein and dissolve it in 1.5% sodium hydroxide solution, and the ratio of silkworm chrysalis protein to sodium hydroxide is 1.0:0.05. .

[0025] The process of producing pupa protein spinning solution by the alkylation reaction of the present invention is to add silkworm pupa protein to 0.5‰ hydrogen peroxide at a certain temperature for initiation, and then add acrylamide according to the ratio of silkworm pupa protein: acrylamide of 1.0:0.05. After the carbamoyl ethylation reaction, the pupa protein spinning solution was obtai...

Embodiment 3

[0031] A method for manufacturing short protein fibers, which is characterized in that it includes the following production steps: dissolving, alkylation reaction to prepare pupa protein spinning solution, coagulation molding, acetalization treatment, water flow, desulfurization, water washing, pickling and water washing, and Oil, tumble dry.

[0032] The dissolving process of the present invention is to take a certain amount of silkworm chrysalis protein and dissolve it in 1% sodium hydroxide solution, and the ratio of silkworm chrysalis protein to sodium hydroxide is 1.0:0.10. .

[0033] The process of preparing pupae protein spinning solution by the alkylation reaction of the present invention is to add silkworm pupae protein to 0.8‰ hydrogen peroxide at a certain temperature for initiation, and then add acrylamide according to the ratio of silkworm pupae protein: acrylamide of 1.0:0.10. After the carbamoyl ethylation reaction, the pupa protein spinning solution was obtain...

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Abstract

The invention relates to a method to produce filature-industry material. It provides a process that use chrysalides albumen filature liquid and fibrin xanthate ester to spin excellent albumen soy fiber by the mode of injection before spinning and the principle of static admixture. It contains plasm, chrysalides albumen, vitriol, NaOH, carbon bisulfide, formaldehyde glutaraldehyde and propylene acyl-amine. The production is soft and its color is golden. In short, it remains favorable weaving ability.

Description

Technical field: [0001] The invention relates to a method for manufacturing novel textile industry materials, in particular to a method for manufacturing protein short fibers. Background technique: [0002] At present, the technology of using silkworm chrysalis protein spinning solution and cellulose to produce viscose filaments is mature, but due to the limited scope of application of viscose filaments, it can only be interwoven with other filaments such as polyester filaments, silk, etc. Used in silk and other fields, it cannot be blended with other staple fibers such as wool, cotton, hemp, polyester staple fiber, viscose staple fiber, etc., which affects the scope of use of silkworm chrysalis protein spinning solution and cellulose as materials in the textile industry. Invention content: [0003] The object of the present invention is to provide a method for producing short fibers by using silkworm chrysalis protein spinning solution and cellulose, the protein short fib...

Claims

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Application Information

Patent Timeline
23 Feb 2005
Publication
CN1584146A
IPC
D01D5/06; D01F4/00
Inventors
冯涛; 刘忠