New technique for synthesizing 2-alkoxyl propylene
A technology of alkoxypropene and process, which is applied in the field of new synthetic process of 2-alkoxypropene, can solve the problems of many side reactions, difficult separation, high equipment requirements, etc., and achieve simple operation, simplified reaction process, high selectivity Good results
Inactive Publication Date: 2005-08-31
ZHEJIANG UNIV +1
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The advantage of this method is that the reaction conversion rate is high and the operation is simple. The disadvantage is that the reaction needs to be carried out at high temperature, electric heating is required, there are many side reactions, the separation is difficult, and the requirements for equipment are also high.
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[0014] The present invention is described in detail below in conjunction with embodiment.
[0015] In a 1m-long tower reactor filled with 180g of acidic material, dialkoxypropane is fed from the bottom of the tower with a pump at a flow rate of 90 g / hour, the temperature at the bottom of the tower is controlled at 120 ° C, and the pressure is controlled at 2 atm. The 2-alkoxypropene was collected.
[0016] Example
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Abstract
Description
technical field [0001] The invention relates to a new synthesis process of 2-alkoxypropene. Background technique [0002] 2-Alkoxypropene is an important pharmaceutical and chemical raw material. Because it has both double bonds and ether bonds, its chemical properties are very active. It is often used as a solvent and auxiliary agent in the paint, textile and leather industries, and also as a key intermediate in the synthesis of medicine, food and feed. Among them, 2-methoxypropene is the most important and widely used alkenyl ether compound, which is used for the synthesis of clarithromycin, pseudoionone, ionone, isophytol, vitamin A, vitamin E, vitamin K2 and other medicines. It is a key intermediate of chemical, chemical and feed products, and has very important uses in industrial production. [0003] There are two methods for synthesizing 2-alkoxypropene: alkyne alcohol condensation and ketal cracking. Among them, the aldol condensatio...
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Patent Type & Authority Applications(China)
IPC IPC(8): C07C41/18C07C43/15
Inventor 李浩然王从敏崔伟胡兴邦姜辉邓东顺徐林祥叶志翔
Owner ZHEJIANG UNIV
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