Method for producing aluminium hydrogen sulfate
A technology of aluminum bisulfate and its production method, which is applied in the direction of aluminum sulfate, aluminum sulfur compounds, etc., can solve the problems of complex control conditions, improper condition control, and difficulty in obtaining products in the synthesis reaction of aluminum bisulfate, so as to meet the needs of the domestic market and reduce the The effect of using cost and production method is simple and feasible
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Embodiment 1
[0033] The production method of aluminum bisulfate of the present invention, at first calculate the theoretical consumption of required sulfuric acid and aluminum sulfate reactant according to the molecular composition of aluminum bisulfate, carry out synthetic reaction with the excess sulfuric acid and aluminum sulfate that actual consumption is greater than theoretical consumption, will The final reaction solution is successively filtered and washed, cooled to crystallize, crystallized and separated, and dried to obtain aluminum bisulfate products, specifically:
[0034] Aluminum bisulfate is AlH(SO 4 ) 2 ·xH 2 O, the actual amount of sulfuric acid is 3.5 times of the theoretical amount;
[0035] Aluminum bisulfate as Al 2 h 2 (SO 4 ) 4 ·yH 2 O, the actual consumption of sulfuric acid is 3.3 times of the theoretical consumption;
[0036] Aluminum bisulfate as Al 4 h 2 (SO 4 ) 7 ·zH 2 O, the actual amount of sulfuric acid is 3.0 times the theoretical amount.
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Embodiment 2
[0040] The production method of aluminum bisulfate of the present invention, at first calculate the theoretical consumption of required sulfuric acid and aluminum sulfate reactant according to the molecular composition of aluminum bisulfate, carry out synthetic reaction with the excess sulfuric acid and aluminum sulfate that actual consumption is greater than theoretical consumption, will The final reaction solution is successively filtered and washed, cooled to crystallize, crystallized and separated, and dried to obtain aluminum bisulfate products, specifically:
[0041] Aluminum bisulfate is AlH(SO 4 ) 2 ·xH 2 O, the actual consumption of sulfuric acid is 3.2 times of the theoretical consumption;
[0042] Aluminum bisulfate as Al 2 h 2 (SO 4 ) 4 ·yH 2 O, the actual amount of sulfuric acid is 2.8 times of the theoretical amount;
[0043] Aluminum bisulfate as Al 4 h 2 (SO 4 ) 7 ·zH 2 O, the actual amount of sulfuric acid is 2.9 times of the theoretical amount. ...
Embodiment 3
[0047]The production method of aluminum bisulfate of the present invention, at first calculate the theoretical consumption of required sulfuric acid and aluminum hydroxide reactant according to the molecular composition of aluminum hydrogen sulfate, carry out synthesis reaction with the excess sulfuric acid and aluminum hydroxide that actual consumption is greater than theoretical consumption , the final reaction solution is sequentially filtered and washed, cooled to crystallize, crystallized and separated, and dried to obtain an aluminum bisulfate product, specifically:
[0048] Aluminum bisulfate is AlH(SO 4 ) 2 ·xH 2 O, the actual consumption of sulfuric acid is 3.6 times of the theoretical consumption;
[0049] Aluminum bisulfate as Al 2 h 2 (SO 4 ) 4 ·yH 2 O, the actual consumption of sulfuric acid is 3.2 times of the theoretical consumption;
[0050] Aluminum bisulfate as Al 4 h 2 (SO 4 ) 7 ·zH 2 O, the actual amount of sulfuric acid is 2.8 times the theore...
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