Dyed layer forming radiation linear combination, colour filter and liquid crystal display screen
A composition and radiation-sensitive technology, applied in the direction of optical filters, nonlinear optics, photosensitive materials for optomechanical devices, etc.
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Synthetic example 1
[0286] In a flask equipped with a cooling tube and a stirrer, add 1 part by weight of 2,2'-azobis(2,4-dimethylvaleronitrile) and 200 parts by weight of propylene glycol monomethyl ether acetate, and then add 15 parts by weight of methacrylic acid, 15 parts by weight of styrene, 35 parts by weight of benzyl methacrylate, 10 parts by weight of glycerol monomethacrylate, 25 parts by weight of N-phenylmaleimide and chain transfer agent α- After replacing 2.5 parts by weight of methylstyrene dimer with nitrogen, the mixture was slowly stirred, the temperature of the reaction solution was raised to 80° C., and the temperature was maintained for 3 hours for polymerization. Then, the temperature of the reaction solution was raised to 100°C, 0.5 parts by weight of 2,2'-azobis(2,4-dimethylvaleronitrile) was added, and polymerization was carried out for 1 hour to obtain (B) an alkali-soluble resin Solution (solid content concentration=33.0% by weight).
[0287] Mw=17,000 and Mn=8,000 of...
Synthetic example 2
[0289] In a flask equipped with a cooling tube and a stirrer, add 1 part by weight of 2,2'-azobis(2,4-dimethylvaleronitrile) and 200 parts by weight of propylene glycol monomethyl ether acetate, and then add 15 parts by weight of methacrylic acid, 15 parts by weight of styrene, 30 parts by weight of benzyl methacrylate, 15 parts by weight of glycerol monomethacrylate, 25 parts by weight of N-phenylmaleimide and chain transfer agent α- After replacing 2.5 parts by weight of methylstyrene dimer with nitrogen, the mixture was slowly stirred, the temperature of the reaction solution was raised to 80° C., and the temperature was maintained for 3 hours for polymerization. Then, the temperature of the reaction solution was raised to 100°C, 0.5 parts by weight of 2,2'-azobis(2,4-dimethylvaleronitrile) was added, and polymerization was carried out for 1 hour to obtain (B) an alkali-soluble resin solution (solid content concentration=32.9% by weight).
[0290] Mw=19,000 and Mn=9,000 of...
Synthetic example 3
[0292] In a flask equipped with a cooling tube and a stirrer, add 1 part by weight of 2,2'-azobis(2,4-dimethylvaleronitrile) and 200 parts by weight of propylene glycol monomethyl ether acetate, and then add 15 parts by weight of methacrylic acid, 15 parts by weight of styrene, 30 parts by weight of benzyl methacrylate, 10 parts by weight of glycerol monomethacrylate, 30 parts by weight of N-phenylmaleimide and chain transfer agent α- After replacing 2.5 parts by weight of methylstyrene dimer with nitrogen, the mixture was slowly stirred, the temperature of the reaction solution was raised to 80° C., and the temperature was maintained for 3 hours for polymerization. Then, the temperature of the reaction solution was raised to 100°C, 0.5 parts by weight of 2,2'-azobis(2,4-dimethylvaleronitrile) was added, and polymerization was carried out for 1 hour to obtain (B) an alkali-soluble resin Solution (solid content concentration=33.2% by weight).
[0293]Mw=15,000 and Mn=7,000 of ...
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