Method for extracting natural perfume by polybasic lysosome transfer
A natural fragrance and extraction technology, which is applied in the field of preparation of natural fragrance extracts, can solve the problems that fragrance substances cannot be extracted, and it is difficult to obtain natural fragrances, and achieves the effect of convenient method.
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Embodiment 1
[0011] Cumin extract: Dilute acetone with water to prepare 2000 grams of 70% dilute acetone solution, then add 500 grams of propylene glycol, and the multi-component solvent is prepared. Add 500 grams of fennel powder into the flask, install a stirring and reflux device, add multi-component solvents, and then heat and reflux for 2 hours. Wash the filter residue for the first time, gather the filtrate together, and remove part of the acetone and water with a falling film fractionation tower to obtain 800 grams of concentrated solution, the fennel extract with a solid content of more than 12%, has a mild fennel aroma, Slightly sweet, not oily after storage.
Embodiment 2
[0013] Star anise powder extract: Dilute 95% edible ethanol with water, measure it with an ethanol specific gravity meter, prepare 400 grams of 60% dilute ethanol solution, add this dilute ethanol solution to 100 grams of star anise powder, and reflux extraction for 2 hour, filtered after cooling, and the filter residue was reflux extracted with 40 grams of 60% dilute ethanol and 60 grams of propylene glycol for 2 hours, filtered after cooling, and the filter residue was washed with 50 grams of 60% dilute ethanol, and the combined filtrate was partially separated by a falling film fractionation tower. The ethanol and water are distilled off to obtain 100 grams of concentrated liquid, which is the star anise powder extract, with a clear and spicy star anise aroma and sweet taste.
Embodiment 3
[0015] Five-spice powder extract: Dilute methanol with water to prepare 6,000 grams of 80% dilute methanol solution, then add 800 grams of glycerol, and the multi-component solvent is prepared. Add 2000 grams of five-spice powder to the flask, install a stirring and reflux device, add multi-component solvents, then heat and reflux for 1 hour, after the extraction is completed, cool, filter and remove the five-spice powder residue, and wash twice with 1000 grams of 80% dilute methanol Filter residue, filtrate is gathered together, methanol is evaporated with falling film fractionation tower, obtains the concentrated solution of 1400 grams, five-spice powder extract, has the fragrance of complete five-spice powder, and storage is not short-lived.
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