Optical resin film and polarizing plate and liquid crystal display using same
A liquid crystal display, optical resin technology, applied in optics, optical components, nonlinear optics, etc., can solve the problems of light leakage angle of view, inability to improve chromatic aberration, narrowing, etc.
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Embodiment 1
[0356] (formation of film 1)
[0357] To 60 parts of 6-methyl-1,4,5,8-dioxomethylene-1,4,4a,5,6,7,8,8a-octahydronaphthalene (hereinafter abbreviated as MTD), 10 parts of 15% triethylaluminum cyclohexane solution, 5 parts of triethylamine and 10 parts of 20% titanium tetrachloride cyclohexane solution were added as polymerization catalysts. After ring-opening polymerization in cyclohexane, the obtained ring-opened polymer was hydrogenated with a nickel catalyst to produce a polymer solution. The polymer solution was coagulated in isopropanol and dried to produce a powdered resin. The resin had a number average molecular weight of 40,000, its hydrogenation rate was 99.8% or more, and its Tg was 142°C.
[0358] The powdery resin was melted at 250° C. and pelletized. Using a single-screw extruder with a 40-nm fully-flighted screw, the obtained pellets were melt-extruded from a 300-mm-wide T-die, and rolled up with three 300-mm-diameter cooling rolls to produce films. In this p...
Embodiment 2
[0371] Film 1 obtained in Example 1 was freely uniaxially stretched in the conveying direction at 185° C. at a stretch rate of 15% to give a stretched and oriented film. Table 1 shows its optical properties.
[0372] Likewise, Films 2-4 were stretched under the conditions specified in Table 1. Table 1 also shows the optical properties thus obtained.
[0373] In Tables 1 to 3, the numerical values given in columns (A) to (D) each represent the following values.
[0374] (A)Re(450) / Re(550)
[0375] (B)Re(650) / Re(550)
[0376] (C)(Re(450) / Rth(450)) / (Re(550) / Rth(550))
[0377] (D)(Re(650) / Rth(650)) / (Re(550) / Rth(550))
[0378] Film No.
Embodiment 3
[0380]Films 1-4 obtained in Example 1 were freely uniaxially stretched in the conveying direction at 185° C. at a stretch rate of 25%. Next, the films were released at 25% in the conveying direction to give stretched and oriented films. Table 2 shows the stretching conditions and optical properties.
[0381]
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