Light-curing, self-etching, one-component dental adhesive containing nanoparticles
A technology of adhesive and photohardening, applied in dental preparations, dentistry, dental prosthesis, etc., can solve problems such as adhesive hardening hindrance, and achieve long-term stability, high intrinsic strength, and good film-forming properties
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[0032] 2. Measurement of bond shear strength
[0033] The effect of acidic monomers in adhesive formulation was examined by determining the bond shear strength on dentin and enamel. Human teeth were used which were preserved in a 0.5% chloramine T-solution for up to 3 months after extraction. The teeth were carefully rinsed under running water before applying the adhesion test. The day before the application of the adhesion test, the teeth were buried with TECHNOVIT 4001 in a cylindrical rubber membrane and each tooth was on abutting surfaces. These teeth were ground by wet grinding with 80.240 grit SiC paper and finally 600 grit SiC paper to such an extent that sufficient dentin and enamel surfaces were exposed for use with 2.38mm diameter plastic Cylindrical bonding. After rinsing with desalinated water, the teeth are air-dried. The formulations made from Examples 2A-F were applied to tooth surfaces in three coats with a brush, dried in a press...
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