Silver-containing antibacterial viscose fiber and its preparing method
A technology of viscose fiber and antibacterial fiber, which is applied in the field of preparation of silver-based antibacterial viscose fiber, which can solve the problems of decreased antibacterial performance, poor antistatic performance, and failure to achieve antibacterial purposes, etc.
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Embodiment 1
[0032] (1) Impregnation: The immersion temperature is 45°C, the concentration of lye is 225g / L, and the immersion time is 70 minutes.
[0033] (2) Pressing: the content of methyl fiber is 26%, and the content of sodium hydroxide is 14.5%.
[0034] (3) Mature: temperature 55°C.
[0035] (4) Yellowing: the amount of carbon disulfide is 36%, the initial temperature is 32°C, the final temperature is 40°C, and the time is 150 minutes
[0036] (5) Dissolution: the content of methyl fiber is 8.5%, and the content of sodium hydroxide is 5.3%.
[0037] (6) Spinning: acid bath composition: sulfuric acid 125g / L sodium sulfate 330g / L zinc sulfate 10.5g / L temperature 51°C.
[0038] (7) The amount of nano-silver particles added: 0.6‰ (based on the amount of methyl fiber). Particle size: 55 nm.
[0039] (8) Finished product quality: antibacterial value: 3.57 sterilization value: 1.38
[0040] Dry breaking strength: 2.26CN / dtex Wet breaking strength: 1.34CN / dtex
[0041] Dry elongation ...
Embodiment 2
[0044] (1) Impregnation: The impregnation temperature is 50°C, the concentration of lye is 235g / L, and the impregnation time is 60 minutes.
[0045] (2) Pressing: the content of methyl fiber is 27%, and the content of sodium hydroxide is 15%.
[0046] (3) Mature: temperature 50°C.
[0047] (4) Yellowing: the amount of carbon disulfide is 38%, the initial temperature is 35°C, the final temperature is 42°C, and the time is 45 minutes.
[0048] (5) Dissolution: the content of methyl cellulose is 9.00%, and the content of sodium hydroxide is 5.70%.
[0049] (6) Spinning: acid bath composition: sulfuric acid 130g / L, sodium sulfate 335g / L, zinc sulfate 11g / L, temperature 50°C.
[0050] (7) The amount of nano-silver particles added: 2‰ (based on the amount of methyl fiber). Particle size: 60 nm.
[0051] (8) Finished product quality: antibacterial value: 3.68 sterilization value: 1.57
[0052] Dry breaking strength: 2.35CN / dtex Wet breaking strength: 1.41CN / dtex
[0053]Dry elo...
Embodiment 3
[0056] (1) Impregnation: The immersion temperature is 55°C, the concentration of lye is 235g / L, and the immersion time is 60 minutes.
[0057] (2) Pressing: the content of methyl fiber is 28%, and the content of sodium hydroxide is 15.5%.
[0058] (3) Mature: Temperature 45°C
[0059] (4) Yellowing: the amount of carbon disulfide is 40%, the initial temperature is 35°C, the final temperature is 40°C, and the time is 40 minutes.
[0060] (5) Dissolution: the content of methyl fiber is 9.5%, and the content of sodium hydroxide is 6.0%.
[0061] (6) Spinning: acid bath composition: sulfuric acid 135g / L, sodium sulfate 340g / L, zinc sulfate 11.5g / L, temperature 49°C.
[0062] (7) The amount of nano-silver particles added: 4‰ (based on the amount of methyl fiber). Particle size: 60 nm.
[0063] (8) Finished product quality: antibacterial value: 3.85 sterilization value: 1.73
[0064] Dry breaking strength: 2.41CN / dtex Wet breaking strength: 1.43CN / dtex
[0065] Dry elongation ...
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