Silver-containing antibacterial viscose fiber and its preparing method

A technology of viscose fiber and antibacterial fiber, which is applied in the field of preparation of silver-based antibacterial viscose fiber, which can solve the problems of decreased antibacterial performance, poor antistatic performance, and failure to achieve antibacterial purposes, etc.

Active Publication Date: 2007-03-28
吉林化纤股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although this kind of fiber has antibacterial properties, it also has the irreparable defects of synthetic fibers, namely: when used in clothing, sanitary materials, and bedding, it has poor hygroscopicity and antistatic properties, and it is antibacterial after being subjected to high temperatures, chemicals, and repeated washing. The antibacterial properties are reduced, and the real antibacterial purpose cannot be achieved. At the same time, the drug will also cause certain allergic reactions and affect the performance of taking; even if inorganic antibacterial agents are used, most of them contain heavy metal ions, which are harmful to the human body. Silver-based antibacterial agents are less harmful to the human body among antibacterial agents, and are beneficial to the human body when used in small amounts, and have a strong ability to kill Staphylococcus aureus and Escherichia coli

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] (1) Impregnation: The immersion temperature is 45°C, the concentration of lye is 225g / L, and the immersion time is 70 minutes.

[0033] (2) Pressing: the content of methyl fiber is 26%, and the content of sodium hydroxide is 14.5%.

[0034] (3) Mature: temperature 55°C.

[0035] (4) Yellowing: the amount of carbon disulfide is 36%, the initial temperature is 32°C, the final temperature is 40°C, and the time is 150 minutes

[0036] (5) Dissolution: the content of methyl fiber is 8.5%, and the content of sodium hydroxide is 5.3%.

[0037] (6) Spinning: acid bath composition: sulfuric acid 125g / L sodium sulfate 330g / L zinc sulfate 10.5g / L temperature 51°C.

[0038] (7) The amount of nano-silver particles added: 0.6‰ (based on the amount of methyl fiber). Particle size: 55 nm.

[0039] (8) Finished product quality: antibacterial value: 3.57 sterilization value: 1.38

[0040] Dry breaking strength: 2.26CN / dtex Wet breaking strength: 1.34CN / dtex

[0041] Dry elongation ...

Embodiment 2

[0044] (1) Impregnation: The impregnation temperature is 50°C, the concentration of lye is 235g / L, and the impregnation time is 60 minutes.

[0045] (2) Pressing: the content of methyl fiber is 27%, and the content of sodium hydroxide is 15%.

[0046] (3) Mature: temperature 50°C.

[0047] (4) Yellowing: the amount of carbon disulfide is 38%, the initial temperature is 35°C, the final temperature is 42°C, and the time is 45 minutes.

[0048] (5) Dissolution: the content of methyl cellulose is 9.00%, and the content of sodium hydroxide is 5.70%.

[0049] (6) Spinning: acid bath composition: sulfuric acid 130g / L, sodium sulfate 335g / L, zinc sulfate 11g / L, temperature 50°C.

[0050] (7) The amount of nano-silver particles added: 2‰ (based on the amount of methyl fiber). Particle size: 60 nm.

[0051] (8) Finished product quality: antibacterial value: 3.68 sterilization value: 1.57

[0052] Dry breaking strength: 2.35CN / dtex Wet breaking strength: 1.41CN / dtex

[0053]Dry elo...

Embodiment 3

[0056] (1) Impregnation: The immersion temperature is 55°C, the concentration of lye is 235g / L, and the immersion time is 60 minutes.

[0057] (2) Pressing: the content of methyl fiber is 28%, and the content of sodium hydroxide is 15.5%.

[0058] (3) Mature: Temperature 45°C

[0059] (4) Yellowing: the amount of carbon disulfide is 40%, the initial temperature is 35°C, the final temperature is 40°C, and the time is 40 minutes.

[0060] (5) Dissolution: the content of methyl fiber is 9.5%, and the content of sodium hydroxide is 6.0%.

[0061] (6) Spinning: acid bath composition: sulfuric acid 135g / L, sodium sulfate 340g / L, zinc sulfate 11.5g / L, temperature 49°C.

[0062] (7) The amount of nano-silver particles added: 4‰ (based on the amount of methyl fiber). Particle size: 60 nm.

[0063] (8) Finished product quality: antibacterial value: 3.85 sterilization value: 1.73

[0064] Dry breaking strength: 2.41CN / dtex Wet breaking strength: 1.43CN / dtex

[0065] Dry elongation ...

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Abstract

The invention relates to a manufacture method for antibiotic mucilage glue fiber that uses nanometer silver as additive. The method includes the following steps: mixing grains, making glue, spinning, beaming, cutting, refining, drying, packing nanometer silver antibiotic agent; mixing grains, making glue, spinning, beaming, cutting, refining, drying and packing antibiotic mucilage glue fiber. It has the advantages of asepsis, strong antibiotic effect, long effecting time and strong dry-wet rigidity.

Description

technical field [0001] The invention relates to the production of antibacterial fibers from cellulose pulp and nano-silver colloid solution, more precisely, the preparation method of silver-based antibacterial viscose fibers. technical background [0002] At present, most of the antibacterial fibers are synthetic fibers, and the antibacterial agents are mainly organic antibacterial agents, which are added through melt spinning or post-finishing. Although this kind of fiber has antibacterial properties, it also has the irreparable defects of synthetic fibers, namely: when used in clothing, sanitary materials, and bedding, it has poor hygroscopicity and antistatic properties, and it is antibacterial after being subjected to high temperatures, chemicals, and repeated washing. The antibacterial properties are reduced, and the real antibacterial purpose cannot be achieved. At the same time, the drug will also cause certain allergic reactions and affect the performance of taking; ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F2/08D01F1/10
Inventor 宋德武郑书华岳福生李振峰范小勇陈达志
Owner 吉林化纤股份有限公司
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