Stick cosmetic and process for producing the same
A technology for cosmetics and rods, applied in the field of rod-shaped cosmetics and its manufacturing, can solve the problems of great influence on strength, decrease in strength, difficulty in maintaining shape, etc., and achieve the effect of less damage to color development and excellent impact strength
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Embodiment 1
[0064] 300 g of ion-exchanged water, 300 g of cetyltrimethylammonium bromide as a surfactant, and 25 g of 0.1 mol / l HCl were added, and stirred at 30° C. for 30 minutes (solution 1). Next, a mixture of 50 g of tetraethylorthosilicate (TEOS) as a source of Si and 50 g of titanium isopropoxide as a source of Ti was added to the above solution 1, and stirred at 30° C. for 2 hours to prepare the mesoporosity. Solution A for material formation. Using this solution A, a stick-shaped cosmetic was prepared by the following mixing composition and the following production method.
[0065] Mix composition:
[0066] Solution A 30.0% by weight
[0067] Prussian blue 24.0% by weight
[0068] Titanium oxide 6.0% by weight
[0069] Kaolin 20.0% by weight
[0070] Boron nitride 20.0% by weight
[0071] The above-mentioned mixed composition was kneaded, and the kneaded product was extruded into a thin wire by an extruder, dried in air at 50° C. for 24 hours, ultrasonically washed with dis...
Embodiment 2
[0073] Dilute 20g of No. 3 sodium silicate (SiO 2 = 29.1%, Na 2 O=9.45%), make it pass through the column that is filled with II+ type cation exchange resin (Amberlite IR-120B) beforehand, recover active carbon dioxide 100g. On the other hand, an aqueous solution in which 5.6 g of octadecyltrimethylammonium chloride was dissolved was prepared, and the above-mentioned active silica gel was added little by little, and the entire amount was added in about 5 hours to prepare a solution for forming a mesoporous material. b. Using this solution B, a stick-shaped cosmetic was prepared by the following mixing composition and the following production method.
[0074] Mix composition:
[0075] Solution B 30.0% by weight
[0076] Prussian blue 14.0% by weight
[0077] Titanium oxide 6.0% by weight
[0078] Kaolin 30.0% by weight
[0079] Boron nitride 20.0% by weight
[0080]Knead the above mixed composition, use an extruder to extrude the kneaded product into a thin thread, dry ...
Embodiment 3
[0082] Dilute 50g of tetraethoxysilane with 50g of ethanol, slowly drop into 50g of polyethylene glycol (average molecular weight 400), mix for 1 hour, then drop into 100g of 0.1N-HCl aqueous solution, mix for 6 hours, to make mesoporous material solution C. Using this solution C, a stick-shaped cosmetic was prepared by the following mixing composition and the following production method.
[0083] Mix composition:
[0084] Solution C 30.0% by weight
[0085] Prussian blue 20.0% by weight
[0086] Titanium oxide 5.0% by weight
[0087] Kaolin 15.0% by weight
[0088] Boron nitride 30.0% by weight
[0089] The above-mentioned mixed composition is kneaded, and the kneaded product is extruded into a thin wire by an extruder, dried at 80°C in the air for 24 hours, and then ultrasonically washed with distilled water for 1 hour, and then Microwave heating (2.45GHz·700W) for 3 minutes produced a light blue rod-shaped cosmetic material with a diameter of 2.0mm.
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