Method for producing homogeneous fine grain titanium materials suitable for ultrasonic inspection

a technology of titanium material and ultrasonic inspection, which is applied in the field of titanium material production methods, can solve the problems of limiting the application of titanium, unsatisfactory noise, and defects in titanium materials, and achieves the effect of reducing the number of defects and improving the quality of titanium materials

Inactive Publication Date: 2005-07-07
GENERAL ELECTRIC CO
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The size of titanium grains and the nature of αTi particle colony structures may influence ultrasonic inspection techniques, methods, and results by creating undesirable noise during ultrasonic inspection.
This noise may hide or mask critical flaws in titanium that may limit applications of the titanium.
While thermomechanical processing techniques that rely on dynamic recrystallization in the α+β temperature range to achieve uniform fine grain (UFG) αTi particles and prevent colony formation have been developed to improve titanium microstructure, defects may remain in the titanium material.
These defects may be undesirable for some titanium material applications.
Thus, the defects should be discovered prior to use of the titanium material in various microstructurally sensitive applications.
While this type of recrystallization has been proposed to improve titanium material microstructure, defects may remain in the titanium material, and these defects may limit applications of the titanium material.
Some of the defects in the titanium material may be difficult to detect using conventional ultrasonic inspection techniques and methods.
Materials forming articles and structures with large, elastically anisotropic grains, such as, but not limited to, cast ingots of steels, titanium alloys, and nickel alloys, are often difficult to evaluate by ultrasonic testing.
The difficulties arise, at least in part to, because sound waves, which are used for ultrasonic inspection, are reflected from grains and grain arrays sharing common elastic behavior, and represent a background “noise.” The generated background noise can mask flaws in the material, and is thus undesirable.
While ultrasonic inspection of most titanium material articles can be preformed with some degree of certainty, the shape, size, configuration, structure, and orientation of the articles, titanium material grains and microstructures formed during a titanium material production method undergoing ultrasonic inspection may impair the ultrasonic inspection.

Method used

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  • Method for producing homogeneous fine grain titanium materials suitable for ultrasonic inspection
  • Method for producing homogeneous fine grain titanium materials suitable for ultrasonic inspection
  • Method for producing homogeneous fine grain titanium materials suitable for ultrasonic inspection

Examples

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example 1

[0036] Titanium material blanks comprising a two-phase titanium alloy (Ti-6242) having a Tpt of about 1000° C were provided. The titanium material blanks were cut from a deformed β-region in a titanium material rod. The dimensions of the titanium material blanks were 100 mm by 100 mm by 200 mm. The β-grain size was in from about 3 mm to about 5 mm. The titanium material microstructure was extended or elongated in a direction of deformation.

[0037] The titanium material blanks were initially heated to a temperature in the β-region (T equal to about 1020° C., dwelling time equal to about 1 hour). The titanium material blanks were then quenched from the temperature of the β-region to create a homogeneous fine grain microstructure in (α+β)-region. Disperse lamellar microstructure was formed and a layer of α-phase titanium was formed disposed around boundaries of the β-grains with a reduced thickness compared to conventional titanium material production methods. This titanium material pr...

example 2

[0039] Titanium material blanks comprising a two-phase titanium alloy (IMI550) were provided. The alloy had a Tpt of about 965° C. for an ingot and a Tpt of about 980° C. for a forging. The titanium material formed as an ingot (billet) with an approximate size of 634 mm by 540 mm was prepared by a titanium material production method that included subjecting the titanium material to a forging in the β-region. This step was followed by heat treatment at about 1200° C., and thereafter by forging and rollforming. This step included settling, forging on the square, and rollforming. A heat treatment step followed with heating at 1140° C. and forging to 390 mm. These steps were followed by cooling in air. Further, the titanium material production method, as embodied by the invention, included a step of heating at Tpt−30° C. and forging to 310 mm, heating at 1060° C., forging to 280 mm, and cooling by air were conducted. Further, the titanium material blank was subjected to heating at Tpt−3...

example 3

[0042] Titanium material blanks comprising a two-phase titanium alloy (VT8-1) were provided, in which the titanium material blanks possessed a Tpt of about 965° C. as an ingot and a Tpt of about 1000° C. as a forging. The ingot, which has a size of about 628 mm by 535 mm, was subjected to a forging in the β-region of titanium. The forging was followed by heat treatment at about 1200° C., and forging that included rollforming, settling, forging on a square, and rollforming. This step was followed by heat treatment at about 1140° C., forging to about 390 mm, and a cooling by air. Further, a heat treatment at about Tpt−30° C. and forging to 310 mm, heating at about 1060° C. and forging to 280 mm followed by cooling in air were also conducted on the titanium material blanks.

[0043] The titanium material blank can then be subjected to heating at about Tpt−30° C. followed by forging. The forging included settling, forging on a square, roll-forming, and forging to 245 mm. After a heat trea...

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Abstract

A titanium material production method for producing homogeneous fine grain titanium material in which the titanium material has a grain size in a range from about 5 μm to about 20 μm. The method comprises providing a titanium material blank; conducting a first heat treatment on the titanium material blank to heat the titanium material blank to a β-range; quenching the titanium material blank from the β-region to the α+β-region; forging the titanium material blank; and conducting a second heat treatment on the titanium material blank. The titanium material production method subjects the titanium material blank to superplasticity conditions during part of the titanium material production method.

Description

BACKGROUND OF THE INVENTION [0001] The invention relates to titanium material production methods. In particular, the invention relates to titanium material production methods that can produce titanium materials suitable for inspection using ultrasonic energy inspection methods and systems. [0002] The production of titanium material with titanium material grain sizes and nature of αTi particle colony structures may be important variables that influence titanium material applications. Further, size of titanium grains and a nature of αTi particle colony structures may influence the ultrasonic noise and ultrasonic inspection in single phase and two-phase titanium alloys and materials, in which the ultrasonic inspection can be used to determine suitability of the titanium material for various applications. The size of titanium grains and the nature of αTi particle colony structures may influence ultrasonic inspection techniques, methods, and results by creating undesirable noise during u...

Claims

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Application Information

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Patent Type & Authority Applications(United States)
IPC IPC(8): C22F1/18
CPCC22F1/183
Inventor BEWLAY, BERNARD PATRICKDEATON, JOHN BRODDUS JR.GILMORE, ROBERT SNEEGIGLIOTTI, MICHAEL FRANCIS XAVIERSALISHCHEV, GENNADY A.KAIBYSHEV, OSKAR A.
Owner GENERAL ELECTRIC CO
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