Ultrasonic treatment chamber for preparing emulsions
a technology of ultrasonic treatment chamber and emulsion, which is applied in the direction of transportation and packaging, mechanical equipment, energy-based chemical/physical/physicochemical processes, etc., can solve the problems of human error, time, energy and money, and the conventional method of mixing phases into emulsions have several problems
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example 1
[0102]In this Example, the ability of the ultrasonic mixing system of the present disclosure to mix an oil phase and aqueous liquid phase to form an oil-in-water type emulsion was analyzed. Specifically, the ability of the ultrasonic mixing system to mix dispersions of mineral oil into a diluted wet wipes solution was analyzed.
[0103]The diluted wet wipe solution included 4.153% (by weight) KIMSPEC AVE® (commercially available from Rhodia, Inc., Cranbury, N.J.) and 95.848% (by weight) purified water. The solution was prepared by mixing the KIMSPEC AVE® into water using a propeller mixer, available from IKA® EUROSTAR, IKA Works Co., Wilmington, N.C.), rotating at a speed of about 540 revolutions per minute (rpm). Four separate samples of the diluted wet wipe solution were prepared. The solution for each sample was delivered to a first inlet port of the ultrasonic mixing system of FIG. 1.
[0104]Additionally, a flow of mineral oil, available as PenrecoO Drakeol® LT mineral oil N.F. from ...
example 2
[0108]In this Example, the ultrasonic mixing system of the present disclosure was used to emulsify an oil phase into a water phase to produce an oil-in-water emulsion. The ability of the ultrasonic mixing system to prepare a stable oil-in-water emulsion was analyzed and compared to an oil-in-water emulsion prepared using a traditional cold mix procedure as described above.
[0109]Three oil-in-water emulsions were prepared. Specifically, the oil-in-water emulsions were prepared by mixing 1 part mineral oil (available as PenrecoO DrakeolO LT mineral oil N.F. from Penreco Co., The Woodlands, Tex.)) to 199 parts water for a mixing period of approximately 2 minutes. The first emulsion sample (Sample 1) was prepared using a propeller mixer (IKA® EUROSTAR, IKA Works, Co., Wilmington, N.C.) and using the standard cold mix batch procedure.
[0110]The other two oil-in-water emulsions (Samples 2 and 3) were prepared in the ultrasonic mixing system of FIG. 1. Specifically, to produce the oil-in-wat...
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