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Glass powder and method of manufacturing the same

a technology of glass powder and manufacturing method, which is applied in the direction of glass making apparatus, manufacturing tools, transportation and packaging, etc., can solve the problems of large number of layers that cannot be substantially stacked as thin film sheets, the size of manufactured powder is micrometer, and the distribution of particle sizes is not uniform,

Inactive Publication Date: 2013-08-15
SAMSUNG ELECTRO MECHANICS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

The present invention pertains to a ceramic material that can be plasticized at a low temperature using glass powder. The technical effect of this invention is the provision of a multi-layered ceramic material that can be easily shaped and formed at low temperatures.

Problems solved by technology

Now, a glass powder formed of five elements or more is generally manufactured through a melt-quenching method, and the manufactured powder has a size of micrometer and non-uniform particle size distribution.
However, since the particle size cannot be reduced to 0.5 μm or less, a large number of layers cannot be substantially stacked as a thin film sheet.
In addition, when a method of forming a sheet is applied, since dispersion of the sheet is deteriorated, a forming sheet cannot be easily manufactured.
However, the crushing method using milling cannot easily crush the powder to a particle size of about 0.5 μm or less, and thus, the powder has a non-uniform particle distribution.

Method used

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  • Glass powder and method of manufacturing the same
  • Glass powder and method of manufacturing the same
  • Glass powder and method of manufacturing the same

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first embodiment

[0068]Hereinafter, a glass powder was manufactured according to manufacturing processes shown in FIG. 2.

[0069]An input amount of starting materials was determined with reference to a solvent of 0.5 mol and 2L, and starting materials of Li, K and Ba and a starting material of B were prepared. The starting material of Li was lithium nitrate, the starting material of K was potassium nitrate, the starting material of Ba was barium acetate, and the starting material of B was boric acid.

[0070]In addition, a starting material of Si was prepared as tetraethyl orthosilicate (TEOS), and the starting materials were weighted to satisfy composition of the glass powder, which is to be manufactured in the present invention.

[0071]Among the starting materials of the prepared Li, K, Ba, B and Si, the starting materials of Li, K, Ba and B were first dissolved in distilled water (900 ml). Here, acetic acid (100 ml) was added. As the acetic acid was added, dissolution of Li, K, Ba and B were accelerated...

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Abstract

Provided are a glass powder represented as aLi2O-bK2O-cBaO-dB2O3-eSiO2 wherein a+b+c+d+e=1, and 0.01≦a≦0.1, 0.01≦b≦0.1, 0.01≦c≦0.1, 0.05≦d≦0.3, and 0.3≦e≦0.7 are satisfied in terms of mol %, a method of manufacturing the same, and a multi-layered ceramic material using the same.Therefore, a nano glass powder having an average particle size of 100 nm or less and uniform particle size distribution can be manufactured using liquid phase deposition, specifically, a sol-gel method.In addition, the glass powder can be used as sintering additives to decrease a sintering temperature by about 100° C. in comparison with conventional glass upon manufacture of a ceramic material such as MLCC and MLCI, which can be sintered at a low temperature, contributing to improvement of dielectric capacity and inductance capacity of the parts and increasing quality coefficient.

Description

CROSS-REFERENCE TO RELATED APPLICATIONS[0001]This application claims the benefit of Korean Patent Application No. 10-2011-0004999 filed with the Korea Intellectual Property Office on Jan. 18, 2011, the disclosure of which is incorporated herein by reference.BACKGROUND OF THE INVENTION[0002]1. Field of the Invention[0003]The present invention relates to a glass powder used in a multi-layered ceramic material and a method of manufacturing the same.[0004]2. Description of the Related Art[0005]In recent times, as mobile telecommunication markets including mobile phones grown, demands of ceramics are being increased as materials for electronic circuit board or multi-layered ceramic electronic parts. As a high conductivity material having a low melting point such as Ag, Cu, etc., is used for internal interconnection circuits, products formed of a ceramic material that can be formed through low-temperature plasticization are also needed.[0006]BaTiO3, Ba(Ca)TiO3, BaTi4O9, etc., are used as ...

Claims

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Application Information

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Patent Type & Authority Applications(United States)
IPC IPC(8): C03C3/089
CPCC03C1/006C03C3/064C03C3/089C03C12/00Y10T428/2982C04B2235/365B82Y30/00B82Y40/00C03C14/00C04B35/00C03C3/078C03B37/00C03C8/02
Inventor AN, SUNGYONGHAHN, JINWOOKIM, JEONGWOOK
Owner SAMSUNG ELECTRO MECHANICS CO LTD