Aqueous ink composition for writing instrument
a writing instrument and composition technology, applied in the field of writing instruments, can solve the problems of disadvantageous impairment of the flow stability of ink, clogging due to further accumulation of aggregation, and the accumulation of microcapsule pigment around the ball, and achieve the effect of excellent stability of ink flow
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production example 1
[0082]As an oil phase solution, while 17 parts of triethylene glycol distearate (ESTEPEARL 30, melting point: 44 to 51° C., manufactured by Nikko Chemicals Co., Ltd.) was warmed to 65° C., 4 parts of titanium oxide (CR-93, manufactured by Ishihara Sangyo Kaisha, Ltd.) was added thereto and dispersed well. Next, 4 parts of methyl ethyl ketone was added, and 7 parts of a trimethylolpropane-modified product of xylylene diisocyanate (D-110N, manufactured by Mitsui Chemicals, Inc.) were further added. The solution was stirred at 65° C.
[0083]As an aqueous phase solution, 15 parts of polyvinyl alcohol (PVA-205, manufactured by Kuraray Co., Ltd.) was dissolved in 600 parts of distilled water warmed to 65° C., and the above-mentioned oil phase solution was added to this solution, and 6 parts of hexamethylene diamine was further added. The solution mixture was subjected to emulsification and mixing to complete polymerization.
[0084]The formed dispersion was centrifuged to recover microcapsules...
production example 2
[0085]Microcapsule pigments (Particles 2) were obtained in the same manner as in Production Example 1 described above, except that the triethylene glycol distearate of Production Example 1 was replaced with the same amount of ethylene glycol distearate (ESTEPEARL 10V, melting point: 58 to 65° C., manufactured by Nikko Chemicals Co., Ltd.). The average particle diameter of Production Example 2 (Particles 2) was 2.8 μm.
production example 3
[0086]Microcapsule pigments (Particles 3) were obtained in the same manner as in Production Example 1 described above, except that the triethylene glycol distearate of Production Example 1 was replaced with the same amount of glycerin monostearate (RHEODOL MS-50, melting point: 55 to 65° C., manufactured by Kao Corporation). The average particle diameter of Production Example 3 (Particles 3) was 3.2 μm.
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