Denatured bamboo pulp viscose short fiber and its production process
A viscose staple fiber and production process technology, applied in the direction of man-made filament in cellulose solution, stretch spinning, etc., can solve the problems of low fiber strength, allergic reaction, etc., achieve low sulfur content, high cleanliness, good quality effect
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Examples
Embodiment 1
[0029] (1) Impregnation: Bamboo pulp is sent into the impregnation barrel to feed meal, impregnate, temperature: 49 ℃, time 60 minutes, the concentration of alkali: 220g / L, denaturant V-388 consumption: 0.5% (p-methyl cellulose).
[0030] (2) Press and crush with AB72 press machine. The pulverized raw material is aged with copper at the aging outlet, the temperature is 49°C, and the viscosity is 48mp;
[0031] (3), yellowing: carbon disulfide adds 32% to methyl cellulose, the yellowing time is 24 minutes, temperature 18 ℃, adds denaturant 0.7% (to methyl cellulose) in dissolving.
[0032] (4), spinning: in spinning machine
[0033] Acid bath: first bath: acid bath with spinning bath liquid, acid bath temperature: 48°C, acid bath drop: 6g / L;
[0034] Second bath: temperature 65°C, sulfuric acid concentration: 55g / L, sodium sulfate concentration: 120g / L.
[0035] (5) Drafting:
[0036] Drafting with drafting machine, total draft: 2.7 times, spinneret draft: 1.6 times
[003...
Embodiment 2
[0042] (1) Impregnation: Bamboo pulp is sent into the impregnation barrel to feed meal, impregnate, temperature: 49 ℃, time 60 minutes, the concentration of alkali: 220g / L, denaturant V-388 consumption: 0.5% (p-methyl cellulose).
[0043] (2), squeezing aging: crushing with AB72 type squeezing machine, the raw material after pulverization is aging with aging export copper sticking, temperature 50 ℃, viscosity is 48mp;
[0044] (3), yellowing: technical condition: carbon disulfide adds 32% to methyl cellulose, and the yellowing time is 26 minutes, and 25 ℃ of temperatures add denaturant 0.9% (to methyl cellulose) in dissolving.
[0045] (4), spinning: in spinning machine
[0046] Acid bath: first bath: acid bath with spinning bath liquid, acid bath temperature: 49°C, acid bath drop: 6g / L;
[0047] Second bath: temperature 68°C, sulfuric acid concentration: 55g / L, sodium sulfate concentration: 120g / L.
[0048] (5) Drafting:
[0049] Drafting with drafting machine, total draft...
Embodiment 3
[0055] (1) Impregnation: bamboo pulp is sent into the impregnation container to feed meal, impregnate, temperature: 49 ℃, the time 60 minutes, the concentration of alkali: 220g / L, denaturant V-388 consumption: 0.5% (paramethylcellulose).
[0056] (2) Squeeze aging: press and pulverize with AB72 type extruder, and the raw material after pulverization is aged with copper at the exit of aging, the temperature is 51°C, and the viscosity is 48mp;
[0057] (3) Yellowing: the addition of carbon disulfide to methyl cellulose is 32%, the yellowing time is 28 minutes, the temperature is 35°C, and 1.0% denaturant (to methyl cellulose) is added in the dissolution.
[0058](4), spinning: in spinning machine
[0059] Acid bath: first bath: acid bath with spinning bath liquid, acid bath temperature: 50°C, acid bath drop: 6g / L;
[0060] Second bath: temperature 70°C, sulfuric acid concentration: 55g / L, sodium sulfate concentration: 120g / L
[0061] (5) Drafting:
[0062] Drafting with draft...
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Abstract
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