Preparation method of seaweed antioxidation active component
An anti-oxidant activity and seaweed technology, applied in chemical instruments and methods, compositions for inhibiting chemical changes, anti-toxins, etc., can solve the problems of lack of implementation of international standards, research level only stays at a low level, and few new drug certificates, etc., to achieve Effects of good flow and transfer properties, easy process regulation, and simple method
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Embodiment 1
[0028] (1) Weigh 100 grams of Chlorella pyrenoidosa powder into supercritical CO 2 Extraction kettle, close the extraction kettle;
[0029] (2) Supercritical carbon dioxide extraction process parameters: pressure 35MPa, temperature 40°C, entrainer dosage 1.5ml ethanol / g material, CO 2 The flow rate is 20L / h, and the pressure and flow rate reach the predetermined value by adjusting the opening degree of the throttle valve and the speed of the carbon dioxide high-pressure pump;
[0030] (3) After reaching the set extraction time of 2.5 hours, the extract is collected, and the extracts in the separation kettle 1 and the separation kettle 2 are combined;
[0031] (4) Vacuum concentration (water bath 40°C) extracts to obtain oily extracts or freeze-dried powdered extracts are the antioxidant active ingredients of seaweed.
[0032] The material collected by supercritical carbon dioxide extraction was concentrated in vacuum at low temperature, and the weight of the extract was meas...
Embodiment 2
[0042] (1) Put 100 grams of Chlorella pyrenoidosa powder into supercritical CO 2 Extraction kettle, close the extraction kettle;
[0043] (2) Set the supercritical carbon dioxide extraction process parameters: pressure 40MPa, temperature 47°C, entrainer dosage 1.5ml ethanol / g material, CO 2 The flow rate is 30L / h, and the pressure and flow rate reach the predetermined value by adjusting the opening degree of the throttle valve and the speed of the carbon dioxide high-pressure pump;
[0044] (3) After reaching the set extraction time of 1.5h, the extract is collected, and the extracts in the separation kettle 1 and the separation kettle 2 are combined;
[0045] (4) Vacuum concentration (water bath 40°C) extracts to obtain oily extracts or freeze-dried powdered extracts are the antioxidant active ingredients of seaweed.
[0046] The material collected by supercritical carbon dioxide extraction was concentrated in vacuum at low temperature, and the weight of the extract was mea...
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