Rumen protection amino acid and preparing method
An amino acid and rumen-passing technology, which can be used in pharmaceutical formulations, medical preparations with inactive ingredients, animal feed, etc., can solve problems such as a certain gap in industrial production and little research on amino acids in ruminants.
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Embodiment 1
[0022] (1) Preparation of granules:
[0023] 50 g of acrylic resin was prepared with absolute ethanol to prepare 500 mL of a 10% protective material solution, mixed with 700 g of methionine to prepare granules, and passed through a 40-mesh sieve to obtain cores.
[0024] (2) Spray the first layer of protective film:
[0025] Put the core obtained in step (1) in the coating pan, preheat the core to 45°C, add 100g of hydrogenated oil directly, and increase the air inlet temperature of the coating pot to 80°C, and adjust the speed to 34r.min -1 After 8 minutes, the hydrogenated oil was melted, and 120 g of calcium stearate was added directly, and continued to heat and rotate for 40 minutes.
[0026] (3) Spray the second layer of protective film:
[0027] Adjust the inlet air temperature to 35°C, the material temperature to 25°C, and the speed to 40r.min -1 , make the atomization pressure of the spray gun 140kPa, spray 1000mL of 3% ethyl cellulose ethanol solution, until there ...
Embodiment 2
[0030] (1) Preparation of granules:
[0031] 60 g of acrylic resin was prepared with absolute ethanol to prepare 600 mL of a 10% protective material solution, mixed with 700 g of lysine to prepare granules, and passed through a 40-mesh sieve to obtain cores.
[0032] (2) Spray the first layer of protective film:
[0033] Put the core obtained in step (1) in the coating pan, preheat the core to 50°C, add 110g of hydrogenated oil directly, and increase the temperature of the air inlet of the coating pot to 93°C, and adjust the speed to 36r.min -1 After 5 minutes, the hydrogenated oil was melted, and 200 g of calcium stearate was added directly, and continued to heat and rotate for 50 minutes.
[0034] (3) Spray the second layer of protective film:
[0035] Adjust the inlet air temperature to 35°C, the material temperature to 27°C, and the speed to 40r.min -1 , make the atomization pressure of the spray gun 140kPa, spray 1000mL of 3% ethyl cellulose ethanol solution, until the...
Embodiment 3
[0038] (1) Preparation of granules:
[0039] Prepare 80g of acrylic resin with absolute ethanol to prepare 800mL of 10% protective material solution, mix with 400g of methionine and 400g of lysine to prepare granules, pass through a 40-mesh sieve to obtain cores.
[0040] (2) Spray the first layer of protective film:
[0041] Put the core obtained in step (1) in the coating pan, preheat the core to 45°C, add 60g of hydrogenated oil directly, and increase the air inlet temperature of the coating pot to 80°C, and adjust the speed to 34r.min -1 After 8 minutes, the hydrogenated oil was melted, and 120 g of calcium stearate was added directly, and continued to heat and rotate for 40 minutes.
[0042] (3) Spray the second layer of protective film:
[0043] Adjust the inlet air temperature to 40°C, the material temperature to 23°C, and the speed to 45r.min -1 , make the atomization pressure of the spray gun 140kPa, spray 1000mL of 5% ethyl cellulose ethanol solution, until there ...
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