Organic particle for inkjet recording sheet and ink jet recording sheet
An organic particle, recording sheet technology, applied in the direction of copying/marking method, printing, etc., can solve the problem of difficulty in obtaining high gloss ink absorption, color development concentration, water resistance, light resistance, yellowing resistance, and inability to obtain ink absorption, etc. question
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[0085] Hereinafter, the present invention will be described with reference to examples, but the present invention is not limited to these examples. In addition, the parts and % shown in an Example represent a weight part and weight% unless otherwise indicated.
[0086]
[0087] Table 1 shows the composition, obtained glass transition temperature (Tg), particle size, and ionicity of the organic particles.
manufacture example 1
[0089] Put 195 parts of deionized water and 2.0 parts of stearyl trimethylammonium chloride into the reaction vessel, raise the temperature to 70°C under nitrogen flow, add 2,2'-azobis(2-amidinopropane) di 0.5 parts of hydrochloride. In addition, 5 parts of 2-hydroxyethyl methacrylate, 60 parts of isobornyl methacrylate, methyl methacrylate 35 parts were emulsified and an emulsified mixture was obtained, and this emulsified mixture was dripped in the reaction container over 4 hours, and it held at the same temperature for further 4 hours after that. As a result, an emulsion composition in which organic particles were dispersed in water was obtained, the non-volatile content was 30%, the pH was 5, the average particle diameter measured by light scattering was 60 nm, and the organic particle aggregation obtained from the DSC curve according to JIS K 7121 The glass transition temperature of the compound is 111°C.
manufacture example 2
[0091] Except putting 195 parts of deionized water and 1.8 parts of stearyl trimethyl ammonium chloride into a reaction container, it manufactured with the composition ratio shown in Table 1 like the manufacture example 1. As a result, an emulsion composition in which organic particles were dispersed in water was obtained. The nonvolatile content was 30%, the pH was 5, the average particle diameter measured by light scattering was 91 nm, and the glass transition temperature of the organic particle polymer was 106°C.
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